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Statements

Subject Item
n2:RIV%2F00216275%3A25310%2F14%3A39897973%21RIV15-MSM-25310___
rdf:type
n19:Vysledek skos:Concept
dcterms:description
MEDSA - N,N-dimethyl-N-metacryloxyethyl-N-(3-sulfopropyl)ammonium betaine as a zwitterionic polar functional monomer in combination with seven crosslinking monomers were used for preparation of capillary monolithic columns suitable for separation of polar compounds in hydrophilic interaction chromatography (HILIC). Ethylene dimethacrylate, tetramethylene dimethacrylate, hexamethylene dimethacrylate, dioxyethylene dimethacrylate, pentaerythritole triacrylate, bisphenol A dimethacrylate, and bisphenol A glycerolate dimethacrylate were used as crosslinking monomers (Fig 1). Columns prepared with dioxyethylene dimethacrylate and bisphenol A glycerolate dimethacrylate showed the efficiency up to 70 000 N/m. Columns provide good repeatability of elution volumes with relative standard deviations lower than 1.3 % on both types of columns. Dual retention mechanism allows the separation in HILIC and RP mode. Capillary monolithic columns, id 0.53 mm, were used in the first dimension of the two-dimensional liquid chromatography for separation of complex mixture of phenolic compounds. Anglická klíčová slova: Monoliths; Characterization; MEDSA MEDSA - N,N-dimethyl-N-metacryloxyethyl-N-(3-sulfopropyl)ammonium betaine as a zwitterionic polar functional monomer in combination with seven crosslinking monomers were used for preparation of capillary monolithic columns suitable for separation of polar compounds in hydrophilic interaction chromatography (HILIC). Ethylene dimethacrylate, tetramethylene dimethacrylate, hexamethylene dimethacrylate, dioxyethylene dimethacrylate, pentaerythritole triacrylate, bisphenol A dimethacrylate, and bisphenol A glycerolate dimethacrylate were used as crosslinking monomers (Fig 1). Columns prepared with dioxyethylene dimethacrylate and bisphenol A glycerolate dimethacrylate showed the efficiency up to 70 000 N/m. Columns provide good repeatability of elution volumes with relative standard deviations lower than 1.3 % on both types of columns. Dual retention mechanism allows the separation in HILIC and RP mode. Capillary monolithic columns, id 0.53 mm, were used in the first dimension of the two-dimensional liquid chromatography for separation of complex mixture of phenolic compounds. Anglická klíčová slova: Monoliths; Characterization; MEDSA
dcterms:title
Zwitterionic monolithic capillary columns for hydrophilic interaction chromatography Zwitterionic monolithic capillary columns for hydrophilic interaction chromatography
skos:prefLabel
Zwitterionic monolithic capillary columns for hydrophilic interaction chromatography Zwitterionic monolithic capillary columns for hydrophilic interaction chromatography
skos:notation
RIV/00216275:25310/14:39897973!RIV15-MSM-25310___
n3:aktivita
n4:P n4:S
n3:aktivity
P(GAP206/12/0398), S
n3:dodaniDat
n8:2015
n3:domaciTvurceVysledku
n6:4487877 n6:9884947
n3:druhVysledku
n16:D
n3:duvernostUdaju
n11:S
n3:entitaPredkladatele
n21:predkladatel
n3:idSjednocenehoVysledku
58026
n3:idVysledku
RIV/00216275:25310/14:39897973
n3:jazykVysledku
n15:eng
n3:klicovaSlova
HILIC, Zwitterionic monolith
n3:klicoveSlovo
n18:HILIC n18:Zwitterionic%20monolith
n3:kontrolniKodProRIV
[A7A755DC47A1]
n3:mistoKonaniAkce
Brno
n3:mistoVydani
Brno
n3:nazevZdroje
CECE 2014: 11th International Interdisciplinary Meeting on Bioanalysis
n3:obor
n9:CB
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
2
n3:projekt
n17:GAP206%2F12%2F0398
n3:rokUplatneniVysledku
n8:2014
n3:tvurceVysledku
Staňková, Magda Jandera, Pavel
n3:typAkce
n13:EUR
n3:zahajeniAkce
2014-10-20+02:00
s:numberOfPages
3
n5:hasPublisher
Ústav analytické chemie AV ČR, v. v. i.
n12:isbn
978-80-904959-2-0
n7:organizacniJednotka
25310