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Statements

Subject Item
n2:RIV%2F00216275%3A25310%2F14%3A39897297%21RIV15-MSM-25310___
rdf:type
skos:Concept n18:Vysledek
dcterms:description
In this study a rapid and easily applicable method for the quantification of 2-ethylhexyl nitrate (2-EHN) in diesel fuel was developed and validated. This method employees Fourier transform infrared spectrometry with attenuated total reflectance (ATR-FTIR). Before the determination of 2-EHN content, could be made to be necessary to analyse the fatty acid methyl esters (FAME) content in diesel fuel in order to prepare the appropriate background solution. Based on the matrix assisted calibration method, the limit of detection was found to be 0.009% w/w for 2-EHN and the limit of quantification 0.025% w/w. The method is linear over the range 0.025-0.300% (w/w), with a correlation coefficient over 0.9998 with satisfactory accuracy, repeatability, and reproducibility. The ATR-FTIR method has been applied to quantify 2-EHN in ten samples of real diesel fuel. Relative standard deviations for all fuel samples were lower than 10%. In this study a rapid and easily applicable method for the quantification of 2-ethylhexyl nitrate (2-EHN) in diesel fuel was developed and validated. This method employees Fourier transform infrared spectrometry with attenuated total reflectance (ATR-FTIR). Before the determination of 2-EHN content, could be made to be necessary to analyse the fatty acid methyl esters (FAME) content in diesel fuel in order to prepare the appropriate background solution. Based on the matrix assisted calibration method, the limit of detection was found to be 0.009% w/w for 2-EHN and the limit of quantification 0.025% w/w. The method is linear over the range 0.025-0.300% (w/w), with a correlation coefficient over 0.9998 with satisfactory accuracy, repeatability, and reproducibility. The ATR-FTIR method has been applied to quantify 2-EHN in ten samples of real diesel fuel. Relative standard deviations for all fuel samples were lower than 10%.
dcterms:title
Fast Determination of 2-Ethylhexyl Nitrate in Diesel Oils by Infrared Spectrometry Fast Determination of 2-Ethylhexyl Nitrate in Diesel Oils by Infrared Spectrometry
skos:prefLabel
Fast Determination of 2-Ethylhexyl Nitrate in Diesel Oils by Infrared Spectrometry Fast Determination of 2-Ethylhexyl Nitrate in Diesel Oils by Infrared Spectrometry
skos:notation
RIV/00216275:25310/14:39897297!RIV15-MSM-25310___
n3:aktivita
n9:I
n3:aktivity
I
n3:cisloPeriodika
January
n3:dodaniDat
n11:2015
n3:domaciTvurceVysledku
n6:8088462 n6:3799794 n6:8428751 n6:6495001 n6:2804417
n3:druhVysledku
n10:J
n3:duvernostUdaju
n17:S
n3:entitaPredkladatele
n15:predkladatel
n3:idSjednocenehoVysledku
16499
n3:idVysledku
RIV/00216275:25310/14:39897297
n3:jazykVysledku
n14:eng
n3:klicovaSlova
GC/MS; FTIR; FAME; Diesel Fuel; 2-Ethylhexyl Nitrate
n3:klicoveSlovo
n8:Diesel%20Fuel n8:FAME n8:2-Ethylhexyl%20Nitrate n8:FTIR n8:GC%2FMS
n3:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n3:kontrolniKodProRIV
[A209F7F3B009]
n3:nazevZdroje
Fuel
n3:obor
n4:CB
n3:pocetDomacichTvurcuVysledku
5
n3:pocetTvurcuVysledku
5
n3:rokUplatneniVysledku
n11:2014
n3:svazekPeriodika
117
n3:tvurceVysledku
Adam, Martin Bajerová, Petra Ventura, Karel Bajer, Tomáš Eisner, Aleš
n3:wos
000327767400001
s:issn
0016-2361
s:numberOfPages
6
n12:doi
10.1016/j.fuel.2013.10.008
n16:organizacniJednotka
25310