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Statements

Subject Item
n2:RIV%2F00216275%3A25310%2F13%3A39896443%21RIV14-MV0-25310___
rdf:type
skos:Concept n5:Vysledek
rdfs:seeAlso
http://www.sciencedirect.com/science/article/pii/S0379073813000133
dcterms:description
Triacetone triperoxide (3,3,6,6,9,9-hexamethyl-1,2,4,5,7,8-hexoxonane, TATP) is nowadays one of the most commonly used improvised explosives. It is prepared by the action of hydrogen peroxide on acetone in an acidic environment. Easily available mineral acids - hydrochloric, sulfuric, nitric and perchloric - are the most often recommended on the extremist web pages dealing with improvised production of explosives. The various TATP producers? choice of acid mainly depends on the author?s experiences and the local availability of the acid. Aknowledge of the kind of acid used for TATP production can help in detecting the person who has made the TATP, or who has committed a criminal act using TATP. Therefore, a capillary isotachophoretic method was developed for determination of residual anions (originating from the acid used during TATP synthesis) in the resulting TATP crystals. This analytical method has proved to be reliable; the acid used for TATP synthesis was correctly identified in all samples analyzed. Triacetone triperoxide (3,3,6,6,9,9-hexamethyl-1,2,4,5,7,8-hexoxonane, TATP) is nowadays one of the most commonly used improvised explosives. It is prepared by the action of hydrogen peroxide on acetone in an acidic environment. Easily available mineral acids - hydrochloric, sulfuric, nitric and perchloric - are the most often recommended on the extremist web pages dealing with improvised production of explosives. The various TATP producers? choice of acid mainly depends on the author?s experiences and the local availability of the acid. Aknowledge of the kind of acid used for TATP production can help in detecting the person who has made the TATP, or who has committed a criminal act using TATP. Therefore, a capillary isotachophoretic method was developed for determination of residual anions (originating from the acid used during TATP synthesis) in the resulting TATP crystals. This analytical method has proved to be reliable; the acid used for TATP synthesis was correctly identified in all samples analyzed.
dcterms:title
Study of TATP: Method for determination of residual acids in TATP Study of TATP: Method for determination of residual acids in TATP
skos:prefLabel
Study of TATP: Method for determination of residual acids in TATP Study of TATP: Method for determination of residual acids in TATP
skos:notation
RIV/00216275:25310/13:39896443!RIV14-MV0-25310___
n5:predkladatel
n6:orjk%3A25310
n3:aktivita
n21:P n21:I
n3:aktivity
I, P(VG20102014032)
n3:cisloPeriodika
1-3
n3:dodaniDat
n14:2014
n3:domaciTvurceVysledku
n15:8356718 n15:4954254
n3:druhVysledku
n19:J
n3:duvernostUdaju
n16:S
n3:entitaPredkladatele
n11:predkladatel
n3:idSjednocenehoVysledku
108764
n3:idVysledku
RIV/00216275:25310/13:39896443
n3:jazykVysledku
n9:eng
n3:klicovaSlova
isotachophoresis; catalyst; residual acid; 8-hexoxonane; 7; 5; 4; 2; 9-Hexamethyl-1; 9; 6; 6; 3; 3; triacetone triperoxide; TATP
n3:klicoveSlovo
n12:2 n12:8-hexoxonane n12:9-Hexamethyl-1 n12:TATP n12:isotachophoresis n12:6 n12:5 n12:7 n12:catalyst n12:9 n12:3 n12:4 n12:triacetone%20triperoxide n12:residual%20acid
n3:kodStatuVydavatele
IE - Irsko
n3:kontrolniKodProRIV
[22107133B624]
n3:nazevZdroje
Forensic Science International
n3:obor
n7:JY
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
2
n3:projekt
n17:VG20102014032
n3:rokUplatneniVysledku
n14:2013
n3:svazekPeriodika
228
n3:tvurceVysledku
Chýlková, Jaromíra Matyáš, Robert
n3:wos
000317829100043
s:issn
0379-0738
s:numberOfPages
4
n10:doi
10.1016/j.forsciint.2013.01.007
n20:organizacniJednotka
25310