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Statements

Subject Item
n2:RIV%2F00216275%3A25310%2F13%3A39896276%21RIV14-GA0-25310___
rdf:type
n8:Vysledek skos:Concept
rdfs:seeAlso
http://link.springer.com/article/10.1007%2Fs10973-012-2347-x
dcterms:description
Crystallization kinetics of chosen compositions from Se-Te glassy system were studied under non-isothermal conditions depending on particle size using differential scanning calorimetry. The purpose of this article is to demonstrate the extent of information accessible by the modern kinetic analysis provided by the differential scanning calorimetry, and to suggest its importance and merit for the development of new, high-tech PCM materials. The crystallization kinetics was described in terms of the nucleation-growth Johnson-Mehl-Avrami model. Complexity of the crystallization process was in this case represented by very closely overlapping consecutive competing surface and bulk nucleation-growth mechanisms. Mutual interactions of both mechanisms as well as all other observed effects were explained in terms of thermal gradients, surface crystallization centers arising from the sample preparation treatments, and changing amount of volume nuclei originating from the combination of pre-nucleation period, and the very glass preparation phase. Accent was laid on the merits resulting from interpretations of characteristic kinetic functions. A new criterion for quick determination of the dominating crystallization mechanism-surface or bulk-was introduced. Crystallization kinetics of chosen compositions from Se-Te glassy system were studied under non-isothermal conditions depending on particle size using differential scanning calorimetry. The purpose of this article is to demonstrate the extent of information accessible by the modern kinetic analysis provided by the differential scanning calorimetry, and to suggest its importance and merit for the development of new, high-tech PCM materials. The crystallization kinetics was described in terms of the nucleation-growth Johnson-Mehl-Avrami model. Complexity of the crystallization process was in this case represented by very closely overlapping consecutive competing surface and bulk nucleation-growth mechanisms. Mutual interactions of both mechanisms as well as all other observed effects were explained in terms of thermal gradients, surface crystallization centers arising from the sample preparation treatments, and changing amount of volume nuclei originating from the combination of pre-nucleation period, and the very glass preparation phase. Accent was laid on the merits resulting from interpretations of characteristic kinetic functions. A new criterion for quick determination of the dominating crystallization mechanism-surface or bulk-was introduced.
dcterms:title
Extended study of crystallization kinetics for Se-Te glasses Extended study of crystallization kinetics for Se-Te glasses
skos:prefLabel
Extended study of crystallization kinetics for Se-Te glasses Extended study of crystallization kinetics for Se-Te glasses
skos:notation
RIV/00216275:25310/13:39896276!RIV14-GA0-25310___
n8:predkladatel
n9:orjk%3A25310
n3:aktivita
n18:P
n3:aktivity
P(GAP106/11/1152), P(LC523)
n3:cisloPeriodika
1
n3:dodaniDat
n5:2014
n3:domaciTvurceVysledku
n13:3988163 n13:1663704
n3:druhVysledku
n20:J
n3:duvernostUdaju
n21:S
n3:entitaPredkladatele
n12:predkladatel
n3:idSjednocenehoVysledku
74375
n3:idVysledku
RIV/00216275:25310/13:39896276
n3:jazykVysledku
n11:eng
n3:klicovaSlova
Se(1-y)Tey; JMA model; DSC; crystallization kinetics
n3:klicoveSlovo
n16:crystallization%20kinetics n16:JMA%20model n16:Se%281-y%29Tey n16:DSC
n3:kodStatuVydavatele
NL - Nizozemsko
n3:kontrolniKodProRIV
[B4D310CE9181]
n3:nazevZdroje
Journal of Thermal Analysis and Calorimetry
n3:obor
n19:CF
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
2
n3:projekt
n15:LC523 n15:GAP106%2F11%2F1152
n3:rokUplatneniVysledku
n5:2013
n3:svazekPeriodika
111
n3:tvurceVysledku
Málek, Jiří Svoboda, Roman
n3:wos
000313207400022
s:issn
1388-6150
s:numberOfPages
11
n14:doi
10.1007/s10973-012-2347-x
n17:organizacniJednotka
25310