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Statements

Subject Item
n2:RIV%2F00216275%3A25310%2F12%3A39895460%21RIV13-GA0-25310___
rdf:type
skos:Concept n5:Vysledek
dcterms:description
On-line two dimensional separation systems combining capillary liquid chromatography with capillary electrophoresis is presented, with special attention to the interface design. Two types of transparent interfaces have been fabricated in the poly methyl methacrylate, with different approaches to the transfer of the fractions from first dimension liquid chromatography separation to the second dimension micellar electrokinetic capillary chromatography separation. The interfaces used for the injection of the mobile phase effluent into the separation capillary are based either on the transverse flow of the background electrolyte, or on the voltage-switching in the tangentially connected channels. The application of both approaches for the separation of selected antioxidants is presented and merits of the interface designs are compared with the recently developed automated off-line twodimensional LCxMEKC separation method. On-line two dimensional separation systems combining capillary liquid chromatography with capillary electrophoresis is presented, with special attention to the interface design. Two types of transparent interfaces have been fabricated in the poly methyl methacrylate, with different approaches to the transfer of the fractions from first dimension liquid chromatography separation to the second dimension micellar electrokinetic capillary chromatography separation. The interfaces used for the injection of the mobile phase effluent into the separation capillary are based either on the transverse flow of the background electrolyte, or on the voltage-switching in the tangentially connected channels. The application of both approaches for the separation of selected antioxidants is presented and merits of the interface designs are compared with the recently developed automated off-line twodimensional LCxMEKC separation method.
dcterms:title
Fast On-line Two-dimensional LCxCE Using Flow and Voltage Gating Interfaces Fast On-line Two-dimensional LCxCE Using Flow and Voltage Gating Interfaces
skos:prefLabel
Fast On-line Two-dimensional LCxCE Using Flow and Voltage Gating Interfaces Fast On-line Two-dimensional LCxCE Using Flow and Voltage Gating Interfaces
skos:notation
RIV/00216275:25310/12:39895460!RIV13-GA0-25310___
n5:predkladatel
n6:orjk%3A25310
n3:aktivita
n18:P
n3:aktivity
P(GAP206/12/0398)
n3:dodaniDat
n11:2013
n3:domaciTvurceVysledku
n8:8169314 n8:2967391 n8:9033327
n3:druhVysledku
n21:D
n3:duvernostUdaju
n15:S
n3:entitaPredkladatele
n14:predkladatel
n3:idSjednocenehoVysledku
136214
n3:idVysledku
RIV/00216275:25310/12:39895460
n3:jazykVysledku
n4:eng
n3:klicovaSlova
capillary electrophoresis; capillary liquid chromatography; Two-dimensional separation
n3:klicoveSlovo
n9:capillary%20electrophoresis n9:Two-dimensional%20separation n9:capillary%20liquid%20chromatography
n3:kontrolniKodProRIV
[81BEB15B6E52]
n3:mistoKonaniAkce
Brno
n3:mistoVydani
Brno
n3:nazevZdroje
CECE 2012: 9th International Interdisciplinary Meeting on Bioanalysis
n3:obor
n22:CB
n3:pocetDomacichTvurcuVysledku
3
n3:pocetTvurcuVysledku
3
n3:projekt
n12:GAP206%2F12%2F0398
n3:rokUplatneniVysledku
n11:2012
n3:tvurceVysledku
Kovaříková, Lenka Fischer, Jan Česla, Petr
n3:typAkce
n17:WRD
n3:zahajeniAkce
2012-10-31+01:00
s:numberOfPages
4
n20:hasPublisher
Ústav analytické chemie AV ČR, v. v. i.
n19:isbn
978-80-904959-1-3
n16:organizacniJednotka
25310