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Statements

Subject Item
n2:RIV%2F00216275%3A25310%2F10%3A39882234%21RIV11-GA0-25310___
rdf:type
n18:Vysledek skos:Concept
dcterms:description
Dehalogenation of halogenated anilines by action of powdered aluminium-nickel alloy in aqueous alkaline solution at room temperature has been studied. The reaction course was monitored by means of H-1 nuclear magnetic resonance (NMR) spectroscopy. The rates of dehalogenation of 4-bromo-, 4-chloro-, 4-fluoro- and 3-chloroaniline were compared under conditions of minimum necessary excess of Al-Ni alloy as reducing agent in edetane buffer medium at pH 10.9. The dehalogenation rates of halogenated anilines decreased in the following order: 3-chloroaniline } 4-bromoaniline a parts per thousand yen 4-chloroaniline } 4-fluoroaniline. On the basis of the results obtained in buffers, the dehalogenation method of aqueous solutions of halogenoanilines was verified using NaOH as the base. Dehalogenation of halogenated anilines by action of powdered aluminium-nickel alloy in aqueous alkaline solution at room temperature has been studied. The reaction course was monitored by means of H-1 nuclear magnetic resonance (NMR) spectroscopy. The rates of dehalogenation of 4-bromo-, 4-chloro-, 4-fluoro- and 3-chloroaniline were compared under conditions of minimum necessary excess of Al-Ni alloy as reducing agent in edetane buffer medium at pH 10.9. The dehalogenation rates of halogenated anilines decreased in the following order: 3-chloroaniline } 4-bromoaniline a parts per thousand yen 4-chloroaniline } 4-fluoroaniline. On the basis of the results obtained in buffers, the dehalogenation method of aqueous solutions of halogenoanilines was verified using NaOH as the base.
dcterms:title
Study of dehalogenation of halogenoanilines using Raney Al-Ni alloy in aqueous medium at room temperature Study of dehalogenation of halogenoanilines using Raney Al-Ni alloy in aqueous medium at room temperature
skos:prefLabel
Study of dehalogenation of halogenoanilines using Raney Al-Ni alloy in aqueous medium at room temperature Study of dehalogenation of halogenoanilines using Raney Al-Ni alloy in aqueous medium at room temperature
skos:notation
RIV/00216275:25310/10:39882234!RIV11-GA0-25310___
n3:aktivita
n4:Z n4:S n4:P
n3:aktivity
P(GP203/07/P248), S, Z(MSM0021627502)
n3:cisloPeriodika
9
n3:dodaniDat
n8:2011
n3:domaciTvurceVysledku
n14:4377931 n14:7769962
n3:druhVysledku
n16:J
n3:duvernostUdaju
n19:S
n3:entitaPredkladatele
n5:predkladatel
n3:idSjednocenehoVysledku
290760
n3:idVysledku
RIV/00216275:25310/10:39882234
n3:jazykVysledku
n15:eng
n3:klicovaSlova
kinetics; ICP-OES; metals; NMR spectroscopy; AOX removal; reductions
n3:klicoveSlovo
n9:ICP-OES n9:AOX%20removal n9:NMR%20spectroscopy n9:reductions n9:kinetics n9:metals
n3:kodStatuVydavatele
AT - Rakouská republika
n3:kontrolniKodProRIV
[96E10DCB4EDE]
n3:nazevZdroje
Monatshefte fur Chemie
n3:obor
n17:DJ
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
3
n3:projekt
n12:GP203%2F07%2FP248
n3:rokUplatneniVysledku
n8:2010
n3:svazekPeriodika
141
n3:tvurceVysledku
Prokeš, Lubomír Krejčová, Anna Weidlich, Tomáš
n3:wos
000281106200013
n3:zamer
n7:MSM0021627502
s:issn
0026-9247
s:numberOfPages
6
n13:organizacniJednotka
25310