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Statements

Subject Item
n2:RIV%2F00216275%3A25310%2F08%3A00007605%21RIV09-GA0-25310___
rdf:type
skos:Concept n17:Vysledek
dcterms:description
The organoantimony(III) difluorides containing Y,C,Y chelating, so called pincer, ligands ([2,6-(YCH2)2C6H3]SbF2; Y = MeO, t-BuO and Me2N ) were prepared by the reaction of corresponding dichlorides ([2,6-(YCH2)2C6H3]SbCl2; Y = MeO, t-BuO and Me2N ) with two equivalents of organotin(IV) fluorinating agents Me3SnF or 2-(Me2NCH2)C6H4Sn(n-Bu2)F, respectively. The structure of organonantimony fluorides was determined both in solution by 1H, 13C and 19F NMR spectroscopy and in the solid state using X-ray diffraction. The organoantimony(III) difluorides containing Y,C,Y chelating, so called pincer, ligands ([2,6-(YCH2)2C6H3]SbF2; Y = MeO, t-BuO and Me2N ) were prepared by the reaction of corresponding dichlorides ([2,6-(YCH2)2C6H3]SbCl2; Y = MeO, t-BuO and Me2N ) with two equivalents of organotin(IV) fluorinating agents Me3SnF or 2-(Me2NCH2)C6H4Sn(n-Bu2)F, respectively. The structure of organonantimony fluorides was determined both in solution by 1H, 13C and 19F NMR spectroscopy and in the solid state using X-ray diffraction. The organoantimony(III) difluorides containing Y,C,Y chelating, so called pincer, ligands ([2,6-(YCH2)2C6H3]SbF2; Y = MeO, t-BuO and Me2N ) were prepared by the reaction of corresponding dichlorides ([2,6-(YCH2)2C6H3]SbCl2; Y = MeO, t-BuO and Me2N ) with two equivalents of organotin(IV) fluorinating agents Me3SnF or 2-(Me2NCH2)C6H4Sn(n-Bu2)F, respectively. The structure of organonantimony fluorides was determined both in solution by 1H, 13C and 19F NMR spectroscopy and in the solid state using X-ray diffraction.
dcterms:title
The synthesis of organoantimony(III) difluorides containing Y,C,Y pincer type ligands using organotin(IV) fluorinating agents. The synthesis of organoantimony(III) difluorides containing Y,C,Y pincer type ligands using organotin(IV) fluorinating agents. The synthesis of organoantimony(III) difluorides containing Y,C,Y pincer type ligands using organotin(IV) fluorinating agents.
skos:prefLabel
The synthesis of organoantimony(III) difluorides containing Y,C,Y pincer type ligands using organotin(IV) fluorinating agents. The synthesis of organoantimony(III) difluorides containing Y,C,Y pincer type ligands using organotin(IV) fluorinating agents. The synthesis of organoantimony(III) difluorides containing Y,C,Y pincer type ligands using organotin(IV) fluorinating agents.
skos:notation
RIV/00216275:25310/08:00007605!RIV09-GA0-25310___
n3:aktivita
n19:Z n19:P
n3:aktivity
P(GA203/07/0468), P(GP203/07/P094), P(LC523), Z(MSM0021620857), Z(MSM0021627501), Z(MSM0021627502)
n3:cisloPeriodika
3
n3:dodaniDat
n14:2009
n3:domaciTvurceVysledku
n6:5347343 n6:1403753 n6:5107962 n6:6345883 n6:8975671
n3:druhVysledku
n11:J
n3:duvernostUdaju
n18:S
n3:entitaPredkladatele
n4:predkladatel
n3:idSjednocenehoVysledku
398793
n3:idVysledku
RIV/00216275:25310/08:00007605
n3:jazykVysledku
n10:eng
n3:klicovaSlova
Antimony; Fluorine; Tin; Chelating ligand; X-ray structure
n3:klicoveSlovo
n5:X-ray%20structure n5:Fluorine n5:Chelating%20ligand n5:Antimony n5:Tin
n3:kodStatuVydavatele
CH - Švýcarská konfederace
n3:kontrolniKodProRIV
[633594D5239B]
n3:nazevZdroje
Journal of Fluorine Chemistry
n3:obor
n8:CA
n3:pocetDomacichTvurcuVysledku
5
n3:pocetTvurcuVysledku
6
n3:projekt
n7:GA203%2F07%2F0468 n7:LC523 n7:GP203%2F07%2FP094
n3:rokUplatneniVysledku
n14:2008
n3:svazekPeriodika
129
n3:tvurceVysledku
Holeček, Jaroslav Růžička, Aleš Dostál, Libor Jirásko, Robert Jambor, Roman Císařová, Ivana
n3:zamer
n16:MSM0021620857 n16:MSM0021627501 n16:MSM0021627502
s:issn
0022-1139
s:numberOfPages
6
n15:organizacniJednotka
25310