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Statements

Subject Item
n2:RIV%2F00216224%3A14740%2F14%3A00073662%21RIV15-MSM-14740___
rdf:type
n11:Vysledek skos:Concept
rdfs:seeAlso
http://ac.els-cdn.com/S0167577X13015838/1-s2.0-S0167577X13015838-main.pdf?_tid=94a14ace-cd43-11e4-958b-00000aacb360&acdnat=1426665266_399e607ceb9d6ceca572da648f05aba9
dcterms:description
The article reports on epsilon-Fe2O3 nanoparticles synthesized in a single step by atmospheric-pressure microwave torch discharge using gaseous precursors only. Morphology and composition of the as-synthesized nanopowder were studied by HR-TEM, XRD, and Mossbauer spectroscopy. In the studied nanopowder, epsilon-Fe2O3 phase (d(xRD)=25 nm, 32 wt%) together with alpha-Fe2O3 and gamma-Fe2O3 phases was found. The characteristic epsilon-Fe2O3 and alpha/gamma-Fe2O3 sextets in the Mossbauer spectra measured at 293 and 5 K confirmed the phase composition of the powder. Compared with the methods currently used for the synthesis of epsilon-Fe2O3 nanoparticles, atmospheric-pressure microwave torch discharge appears as a new synthesis route for obtaining epsilon-Fe2O3 nanoparticles. (C) 2013 Elsevier B.V. All rights reserved. The article reports on epsilon-Fe2O3 nanoparticles synthesized in a single step by atmospheric-pressure microwave torch discharge using gaseous precursors only. Morphology and composition of the as-synthesized nanopowder were studied by HR-TEM, XRD, and Mossbauer spectroscopy. In the studied nanopowder, epsilon-Fe2O3 phase (d(xRD)=25 nm, 32 wt%) together with alpha-Fe2O3 and gamma-Fe2O3 phases was found. The characteristic epsilon-Fe2O3 and alpha/gamma-Fe2O3 sextets in the Mossbauer spectra measured at 293 and 5 K confirmed the phase composition of the powder. Compared with the methods currently used for the synthesis of epsilon-Fe2O3 nanoparticles, atmospheric-pressure microwave torch discharge appears as a new synthesis route for obtaining epsilon-Fe2O3 nanoparticles. (C) 2013 Elsevier B.V. All rights reserved.
dcterms:title
epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch
skos:prefLabel
epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch
skos:notation
RIV/00216224:14740/14:00073662!RIV15-MSM-14740___
n3:aktivita
n18:P n18:I n18:Z
n3:aktivity
I, P(ED1.1.00/02.0068), P(ED2.1.00/03.0086), P(GA106/08/1440), P(GA202/08/0178), P(GAP205/10/1374), Z(AV0Z20410507)
n3:cisloPeriodika
February
n3:dodaniDat
n13:2015
n3:domaciTvurceVysledku
n7:1537539 n7:3437027 n7:8325677
n3:druhVysledku
n15:J
n3:duvernostUdaju
n20:S
n3:entitaPredkladatele
n9:predkladatel
n3:idSjednocenehoVysledku
14886
n3:idVysledku
RIV/00216224:14740/14:00073662
n3:jazykVysledku
n17:eng
n3:klicovaSlova
epsilon-Fe2O3; Nanoparticles; Microwave plasma; Mössbauer spectroscopy
n3:klicoveSlovo
n8:epsilon-Fe2O3 n8:Nanoparticles n8:Microwave%20plasma n8:M%C3%B6ssbauer%20spectroscopy
n3:kodStatuVydavatele
NL - Nizozemsko
n3:kontrolniKodProRIV
[268B9CBD0FDF]
n3:nazevZdroje
Materials Letters
n3:obor
n6:BL
n3:pocetDomacichTvurcuVysledku
3
n3:pocetTvurcuVysledku
6
n3:projekt
n4:ED2.1.00%2F03.0086 n4:GAP205%2F10%2F1374 n4:ED1.1.00%2F02.0068 n4:GA106%2F08%2F1440 n4:GA202%2F08%2F0178
n3:rokUplatneniVysledku
n13:2014
n3:svazekPeriodika
116
n3:tvurceVysledku
David, Bohumil Schneeweiss, Oldřich Jašek, Ondřej Kudrle, Vít Synek, Petr Pizúrová, Naděžda
n3:wos
000331025500100
n3:zamer
n16:AV0Z20410507
s:issn
0167-577X
s:numberOfPages
4
n21:doi
10.1016/j.matlet.2013.11.057
n12:organizacniJednotka
14740