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Statements

Subject Item
n2:RIV%2F00216224%3A14740%2F14%3A00073491%21RIV15-MSM-14740___
rdf:type
n12:Vysledek skos:Concept
dcterms:description
A diode laser thermal vaporization (DLTV) is a sample introduction technique to inductively coupled plasma (ICP), which presents a low-cost alternative to the commercial laser-ablation systems and nebulizers The determination of cobalamin derivatives is of great importance in pharmaceutical analysis. Here we present determination of cobalamins using DLTV ICP MS. Furthermore, the coupling of sensitive DLTV ICP MS with the TLC separation is investigated. Ascending thin layer chromatography (TLC) separation of cobalamins was performed on cellulose – aluminum sheets at ambient temperature in the dark, eluting with solution of n-butanol:ethanol:water (10:3:7). The black ink line was printed over the evolved chromatography sheet, which was used as the substrate for the DLTV technique. The TLC chromatogram was scanned in a simple laboratory-built chamber with the diode laser. A diode laser thermal vaporization (DLTV) is a sample introduction technique to inductively coupled plasma (ICP), which presents a low-cost alternative to the commercial laser-ablation systems and nebulizers The determination of cobalamin derivatives is of great importance in pharmaceutical analysis. Here we present determination of cobalamins using DLTV ICP MS. Furthermore, the coupling of sensitive DLTV ICP MS with the TLC separation is investigated. Ascending thin layer chromatography (TLC) separation of cobalamins was performed on cellulose – aluminum sheets at ambient temperature in the dark, eluting with solution of n-butanol:ethanol:water (10:3:7). The black ink line was printed over the evolved chromatography sheet, which was used as the substrate for the DLTV technique. The TLC chromatogram was scanned in a simple laboratory-built chamber with the diode laser.
dcterms:title
Diode laser thermal vaporisation inductively coupled plasma mass spectrometry of cobalamins Diode laser thermal vaporisation inductively coupled plasma mass spectrometry of cobalamins
skos:prefLabel
Diode laser thermal vaporisation inductively coupled plasma mass spectrometry of cobalamins Diode laser thermal vaporisation inductively coupled plasma mass spectrometry of cobalamins
skos:notation
RIV/00216224:14740/14:00073491!RIV15-MSM-14740___
n4:aktivita
n15:P
n4:aktivity
P(ED1.1.00/02.0068), P(EE2.3.30.0009), P(GAP206/12/0538)
n4:dodaniDat
n14:2015
n4:domaciTvurceVysledku
n7:4550803
n4:druhVysledku
n11:O
n4:duvernostUdaju
n17:S
n4:entitaPredkladatele
n16:predkladatel
n4:idSjednocenehoVysledku
11604
n4:idVysledku
RIV/00216224:14740/14:00073491
n4:jazykVysledku
n10:eng
n4:klicovaSlova
diode laser thermal vaporisation; DLTV; inductively coupled plasma; ICP; cobalamin; thin-layer chromatography; TLC
n4:klicoveSlovo
n6:cobalamin n6:DLTV n6:thin-layer%20chromatography n6:TLC n6:inductively%20coupled%20plasma n6:ICP n6:diode%20laser%20thermal%20vaporisation
n4:kontrolniKodProRIV
[A840AA59E72A]
n4:obor
n9:CB
n4:pocetDomacichTvurcuVysledku
1
n4:pocetTvurcuVysledku
5
n4:projekt
n8:EE2.3.30.0009 n8:GAP206%2F12%2F0538 n8:ED1.1.00%2F02.0068
n4:rokUplatneniVysledku
n14:2014
n4:tvurceVysledku
Preisler, Jan Bednařík, Antonín Tomalová, Iva Foltynová, Pavla Kanický, Viktor
n13:organizacniJednotka
14740