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Statements

Subject Item
n2:RIV%2F00216224%3A14740%2F12%3A00057420%21RIV13-GA0-14740___
rdf:type
skos:Concept n16:Vysledek
dcterms:description
A method for determination of trace elements in submicroliter sample volumes, diode laser thermal vaporization (DLTV) inductively-coupled plasma mass spectrometry (ICP-MS) is presented. Analyte is desorbed from a substrate, such as paper or cellulose containing a suitable absorber, using a continuous-wave diode laser. The laser induces pyrolysis of the substrate and the generated aerosol is carried out into the plasma torch. Unlike laser ablation, DLTV does not require an expensive high-energy pulse laser, which makes it a promising alternative to nebulizers. Analysis of lead in whole blood is demonstrated. Advantages of the method, simplicity, speed, easy archiving and transportation of samples and low cost, are presented. Selection of experimental arrangement and laser wavelength as well as optimization of experimental conditions, e.g., raster type, scan speed, additives etc. was examined. A method for determination of trace elements in submicroliter sample volumes, diode laser thermal vaporization (DLTV) inductively-coupled plasma mass spectrometry (ICP-MS) is presented. Analyte is desorbed from a substrate, such as paper or cellulose containing a suitable absorber, using a continuous-wave diode laser. The laser induces pyrolysis of the substrate and the generated aerosol is carried out into the plasma torch. Unlike laser ablation, DLTV does not require an expensive high-energy pulse laser, which makes it a promising alternative to nebulizers. Analysis of lead in whole blood is demonstrated. Advantages of the method, simplicity, speed, easy archiving and transportation of samples and low cost, are presented. Selection of experimental arrangement and laser wavelength as well as optimization of experimental conditions, e.g., raster type, scan speed, additives etc. was examined.
dcterms:title
Rapid Determination of Lead in Submicroliter Samples of Whole Blood using Diode Laser Thermal Vaporization Rapid Determination of Lead in Submicroliter Samples of Whole Blood using Diode Laser Thermal Vaporization
skos:prefLabel
Rapid Determination of Lead in Submicroliter Samples of Whole Blood using Diode Laser Thermal Vaporization Rapid Determination of Lead in Submicroliter Samples of Whole Blood using Diode Laser Thermal Vaporization
skos:notation
RIV/00216224:14740/12:00057420!RIV13-GA0-14740___
n16:predkladatel
n17:orjk%3A14740
n3:aktivita
n10:S n10:P
n3:aktivity
P(ED1.1.00/02.0068), P(GAP206/12/0538), S
n3:dodaniDat
n14:2013
n3:domaciTvurceVysledku
n12:9236333 n12:2647788 n12:6610528
n3:druhVysledku
n7:O
n3:duvernostUdaju
n5:S
n3:entitaPredkladatele
n13:predkladatel
n3:idSjednocenehoVysledku
164093
n3:idVysledku
RIV/00216224:14740/12:00057420
n3:jazykVysledku
n15:eng
n3:klicovaSlova
lead; blood; laser diode; thermal vaporization; inductively coupled plasma; mass spectrometry; LDTV
n3:klicoveSlovo
n4:lead n4:blood n4:inductively%20coupled%20plasma n4:LDTV n4:thermal%20vaporization n4:mass%20spectrometry n4:laser%20diode
n3:kontrolniKodProRIV
[09211E73AB3B]
n3:obor
n18:CB
n3:pocetDomacichTvurcuVysledku
3
n3:pocetTvurcuVysledku
3
n3:projekt
n9:ED1.1.00%2F02.0068 n9:GAP206%2F12%2F0538
n3:rokUplatneniVysledku
n14:2012
n3:tvurceVysledku
Foltynová, Pavla Preisler, Jan Kanický, Viktor
n8:organizacniJednotka
14740