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Statements

Subject Item
n2:RIV%2F00216224%3A14310%2F97%3A00003795%21RIV08-GA0-14310___
rdf:type
skos:Concept n17:Vysledek
dcterms:description
Reakcí P3N3Cl4(NH2)2 s HCl v acetonitrilu lze připravit ve vysokém výtěžku P3N3Cl5(NH2), jehož krystalová struktura byla určena RTG strukturní analýzou. Při použití diethyletheru nebo dichlormethanu vzniká při této reakci fosfazeniová sůl [P3N3Cl4H(NH2)2]+Cl-. Diskutována byla vibrační spektra obou látek a studováno jejich termické chování. P3N3Cl5(NH2) in high purity and good yield can be obtained by the reaction of P3N3Cl4(NH2)2 with gaseous HCl in acetonitrile If diethylether or dichlormethane is used as a solvent, a salt-like compound [P3N3Cl4H(NH2)2+Cl- is formed as a microcrystalline product instead of P3N3Cl5(NH2). The crystal structure of P3N3Cl5(NH2)was determined by X-ray structure analysis. Vibrational spectra and thermic behavior of both P3N3Cl5(NH2)and [P3N3Cl4H(NH2)2+Cl- are also briefly discussed. P3N3Cl5(NH2) in high purity and good yield can be obtained by the reaction of P3N3Cl4(NH2)2 with gaseous HCl in acetonitrile If diethylether or dichlormethane is used as a solvent, a salt-like compound [P3N3Cl4H(NH2)2+Cl- is formed as a microcrystalline product instead of P3N3Cl5(NH2). The crystal structure of P3N3Cl5(NH2)was determined by X-ray structure analysis. Vibrational spectra and thermic behavior of both P3N3Cl5(NH2)and [P3N3Cl4H(NH2)2+Cl- are also briefly discussed.
dcterms:title
Reakce P3N3Cl4(NH2)2 s HCl: krystalová struktura P3N3Cl5(NH2). The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-. The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-.
skos:prefLabel
The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-. Reakce P3N3Cl4(NH2)2 s HCl: krystalová struktura P3N3Cl5(NH2). The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-.
skos:notation
RIV/00216224:14310/97:00003795!RIV08-GA0-14310___
n4:strany
637
n4:aktivita
n18:P
n4:aktivity
P(GA203/95/1190)
n4:cisloPeriodika
623
n4:dodaniDat
n5:2008
n4:domaciTvurceVysledku
n8:8675058 n8:5708095 n8:4573404 n8:1482823
n4:druhVysledku
n6:J
n4:duvernostUdaju
n7:S
n4:entitaPredkladatele
n10:predkladatel
n4:idSjednocenehoVysledku
811015
n4:idVysledku
RIV/00216224:14310/97:00003795
n4:jazykVysledku
n15:eng
n4:klicovaSlova
preparation; crystal structure; molecular structure; vibrational spectra
n4:klicoveSlovo
n9:preparation n9:vibrational%20spectra n9:crystal%20structure n9:molecular%20structure
n4:kodStatuVydavatele
DE - Spolková republika Německo
n4:kontrolniKodProRIV
[31A4B66A226D]
n4:nazevZdroje
Zeitschrift für anorganische und allgemeine Chemie [Bd. 380 (1971) -]
n4:obor
n12:CA
n4:pocetDomacichTvurcuVysledku
4
n4:pocetTvurcuVysledku
4
n4:projekt
n16:GA203%2F95%2F1190
n4:rokUplatneniVysledku
n5:1997
n4:svazekPeriodika
1997
n4:tvurceVysledku
Alberti, Milan Toužín, Jiří Břínek, Josef Marek, Jaromír
s:issn
0044-2313
s:numberOfPages
5
n14:organizacniJednotka
14310