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Statements

Subject Item
n2:RIV%2F00216224%3A14310%2F08%3A00026062%21RIV11-MSM-14310___
rdf:type
n15:Vysledek skos:Concept
rdfs:seeAlso
www.asms.org
dcterms:description
On-line coupling of column separation techniques with inductively coupled plasma optical emission/mass spectrometry (ICP OES/MS) is routinely used for sensitive, element-selective analysis. Direct linking to ICP usually relies on a nebulizer, which often suffers from reduced separation resolution due to induced liquid flow. Here we report first off-line coupling of capillary electrophoresis (CE) with ICP MS, which is based on eluent deposition on a suitable target followed by laser ablation (LA) and transfer into ICP. The technique is compatible with microcolumn separations, such as capillary electrophoresis or nano liquid chromatography, in terms of both sensitivity and resolution. Furthermore, the fractions collected on the target can be archived and analyzed using other techniques, e.g. MALDI MS or laser-induced fluorescence. On-line coupling of column separation techniques with inductively coupled plasma optical emission/mass spectrometry (ICP OES/MS) is routinely used for sensitive, element-selective analysis. Direct linking to ICP usually relies on a nebulizer, which often suffers from reduced separation resolution due to induced liquid flow. Here we report first off-line coupling of capillary electrophoresis (CE) with ICP MS, which is based on eluent deposition on a suitable target followed by laser ablation (LA) and transfer into ICP. The technique is compatible with microcolumn separations, such as capillary electrophoresis or nano liquid chromatography, in terms of both sensitivity and resolution. Furthermore, the fractions collected on the target can be archived and analyzed using other techniques, e.g. MALDI MS or laser-induced fluorescence.
dcterms:title
Off-Line Coupling of Capillary Electrophoresis to Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Elemental Speciation Off-Line Coupling of Capillary Electrophoresis to Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Elemental Speciation
skos:prefLabel
Off-Line Coupling of Capillary Electrophoresis to Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Elemental Speciation Off-Line Coupling of Capillary Electrophoresis to Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Elemental Speciation
skos:notation
RIV/00216224:14310/08:00026062!RIV11-MSM-14310___
n3:aktivita
n13:P n13:Z
n3:aktivity
P(LC06035), Z(MSM0021622411), Z(MSM0021622412), Z(MSM0021622415)
n3:dodaniDat
n6:2011
n3:domaciTvurceVysledku
n4:2647788 n4:2167301 n4:2257548 n4:6610528 n4:9236333 n4:1700111
n3:druhVysledku
n9:A
n3:duvernostUdaju
n18:S
n3:entitaPredkladatele
n14:predkladatel
n3:idSjednocenehoVysledku
384426
n3:idVysledku
RIV/00216224:14310/08:00026062
n3:jazykVysledku
n10:eng
n3:klicovaSlova
Electrophoresis Capillary; Elemental Analysis; Laser Ablation; Mass Spectrometry; Inductively Coupled Plasma; Speciation
n3:klicoveSlovo
n5:Mass%20Spectrometry n5:Speciation n5:Inductively%20Coupled%20Plasma n5:Laser%20Ablation n5:Elemental%20Analysis n5:Electrophoresis%20Capillary
n3:kodPristupu
n19:V
n3:kontrolniKodProRIV
[FC6953CE2306]
n3:mistoVydani
Denver, USA
n3:objednatelVyzkumneZpravy
ASMS
n3:obor
n7:CB
n3:pocetDomacichTvurcuVysledku
6
n3:pocetTvurcuVysledku
6
n3:projekt
n17:LC06035
n3:rokUplatneniVysledku
n6:2008
n3:tvurceVysledku
Preisler, Jan Peš, Ondřej Foltynová, Pavla Vyhnánek, Radek Vaculovič, Tomáš Kanický, Viktor
n3:verzeVyzkumneZpravy
Proceedings of 56th ASMS Conference
n3:zamer
n16:MSM0021622412 n16:MSM0021622411 n16:MSM0021622415
n11:organizacniJednotka
14310