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Statements

Subject Item
n2:RIV%2F00216224%3A14310%2F08%3A00026051%21RIV10-MSM-14310___
rdf:type
n5:Vysledek skos:Concept
dcterms:description
We present sonochemical synthesis of YFeO3 and Y3Fe5O12 by employing the corresponding mixtures of M(acac)3 precursors. Resulting phase composition of the product can be controlled by the starting stoichiometry of the precursor complexes. Reactions carried out with a 1:1 molar ratio led to amorphous materials that crystallized to perovskite YFeO3 upon calcination. The Y3Fe5O12 garnet phase was produced when a 3:5 molar ratio was employed. SEM was used to examine particle shape, size, and size distribution. The oxide products featured nanoscopic composite particles of a uniform size distribution and nearly spherical shapes with an estimated diameter of 20 nm. TEM study revealed the amorphous structure of the oxide products and the crystalline nature of the calcined phases. HT XRD revealed crystallization of YFeO3 or Y3Fe5O12 on heating and the increase in particle diameter. We present sonochemical synthesis of YFeO3 and Y3Fe5O12 by employing the corresponding mixtures of M(acac)3 precursors. Resulting phase composition of the product can be controlled by the starting stoichiometry of the precursor complexes. Reactions carried out with a 1:1 molar ratio led to amorphous materials that crystallized to perovskite YFeO3 upon calcination. The Y3Fe5O12 garnet phase was produced when a 3:5 molar ratio was employed. SEM was used to examine particle shape, size, and size distribution. The oxide products featured nanoscopic composite particles of a uniform size distribution and nearly spherical shapes with an estimated diameter of 20 nm. TEM study revealed the amorphous structure of the oxide products and the crystalline nature of the calcined phases. HT XRD revealed crystallization of YFeO3 or Y3Fe5O12 on heating and the increase in particle diameter.
dcterms:title
Nanoscopic Yttrium-Iron Garnet and Perovskite by Sonolysis of M(acac)3 Complexes Nanoscopic Yttrium-Iron Garnet and Perovskite by Sonolysis of M(acac)3 Complexes
skos:prefLabel
Nanoscopic Yttrium-Iron Garnet and Perovskite by Sonolysis of M(acac)3 Complexes Nanoscopic Yttrium-Iron Garnet and Perovskite by Sonolysis of M(acac)3 Complexes
skos:notation
RIV/00216224:14310/08:00026051!RIV10-MSM-14310___
n3:aktivita
n9:Z
n3:aktivity
Z(MSM0021622410)
n3:dodaniDat
n4:2010
n3:domaciTvurceVysledku
n7:4700031 n7:8715165 n7:9251189 n7:2274329 n7:2451077 n7:7933665
n3:druhVysledku
n15:D
n3:duvernostUdaju
n6:S
n3:entitaPredkladatele
n20:predkladatel
n3:idSjednocenehoVysledku
381617
n3:idVysledku
RIV/00216224:14310/08:00026051
n3:jazykVysledku
n14:eng
n3:klicovaSlova
Sonochemistry; Iron; Yttrium; Oxides; Garnet; Nanoparticles
n3:klicoveSlovo
n8:Iron n8:Sonochemistry n8:Nanoparticles n8:Oxides n8:Yttrium n8:Garnet
n3:kontrolniKodProRIV
[8C0CF2384D7E]
n3:mistoKonaniAkce
La Grande Motte, Francie
n3:mistoVydani
Basancon, Francie
n3:nazevZdroje
11 th Meeting of the European Society of Sonochemistry
n3:obor
n19:CA
n3:pocetDomacichTvurcuVysledku
6
n3:pocetTvurcuVysledku
6
n3:rokUplatneniVysledku
n4:2008
n3:tvurceVysledku
Zbořil, Radek Moravec, Zdeněk Reichlová, Vendula Pinkas, Jiří Bezdička, Petr Serafimidisová, Aneta
n3:typAkce
n12:WRD
n3:zahajeniAkce
2008-01-01+01:00
n3:zamer
n11:MSM0021622410
s:issn
1350-4177
s:numberOfPages
2
n18:hasPublisher
UTINAM Universite de Franche-Comte
n16:organizacniJednotka
14310