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Statements

Subject Item
n2:RIV%2F00216224%3A14310%2F05%3A00014662%21RIV10-MSM-14310___
rdf:type
n15:Vysledek skos:Concept
dcterms:description
The electrolytic deposition of Ni onto a paraffin-impregnated graphite electrode from supporting chloride electrolyte (0.5 mol dm(-3) NaCl) adjusted to the required pH using dilute HCl is investigated. The effect of electrolyte composition on the Ni electrodeposition is studied using linear sweep voltammetry in the cathodic region. An elimination voltammetry procedure was applied to evaluate the polarization curves. The aim of this work was to deduce the mechanism of Ni reduction in the chloride bath as well as the influence of boric acid on this. Positively-charged NiCl+ ions were found to be the electroactive particles in the Ni reduction mechanism. The strong competition between the NiCl+, Cl- and H+ ions for active sites at the electrode is discussed. Kinetically-controlled adsorption/desorption processes of various species were also confirmed using elimination voltammetry with a linear scan. The electrolytic deposition of Ni onto a paraffin-impregnated graphite electrode from supporting chloride electrolyte (0.5 mol dm(-3) NaCl) adjusted to the required pH using dilute HCl is investigated. The effect of electrolyte composition on the Ni electrodeposition is studied using linear sweep voltammetry in the cathodic region. An elimination voltammetry procedure was applied to evaluate the polarization curves. The aim of this work was to deduce the mechanism of Ni reduction in the chloride bath as well as the influence of boric acid on this. Positively-charged NiCl+ ions were found to be the electroactive particles in the Ni reduction mechanism. The strong competition between the NiCl+, Cl- and H+ ions for active sites at the electrode is discussed. Kinetically-controlled adsorption/desorption processes of various species were also confirmed using elimination voltammetry with a linear scan.
dcterms:title
Influence of boric acid on the electrochemical deposition of Ni Influence of boric acid on the electrochemical deposition of Ni
skos:prefLabel
Influence of boric acid on the electrochemical deposition of Ni Influence of boric acid on the electrochemical deposition of Ni
skos:notation
RIV/00216224:14310/05:00014662!RIV10-MSM-14310___
n3:aktivita
n10:Z
n3:aktivity
Z(MSM0021622412)
n3:cisloPeriodika
2
n3:dodaniDat
n4:2010
n3:domaciTvurceVysledku
n12:3790185 n12:2091690
n3:druhVysledku
n16:J
n3:duvernostUdaju
n13:S
n3:entitaPredkladatele
n6:predkladatel
n3:idSjednocenehoVysledku
524641
n3:idVysledku
RIV/00216224:14310/05:00014662
n3:jazykVysledku
n7:eng
n3:klicovaSlova
Ni electrodeposition; chloride supporting electrolyte; graphite electrode; boric acid; elimination voltammetry
n3:klicoveSlovo
n5:graphite%20electrode n5:chloride%20supporting%20electrolyte n5:Ni%20electrodeposition n5:boric%20acid n5:elimination%20voltammetry
n3:kodStatuVydavatele
CZ - Česká republika
n3:kontrolniKodProRIV
[33E175CC6E8A]
n3:nazevZdroje
JOURNAL OF SOLID STATE ELECTROCHEMISTRY
n3:obor
n11:CG
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
5
n3:rokUplatneniVysledku
n4:2005
n3:svazekPeriodika
10
n3:tvurceVysledku
Oriňáková, Renáta Trnková, Libuše Šupicová, Magdalena Gálová, Miriam Rozik, Roland
n3:zamer
n17:MSM0021622412
s:issn
1432-8488
s:numberOfPages
8
n18:organizacniJednotka
14310