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Statements

Subject Item
n2:RIV%2F00216224%3A14310%2F02%3A00007288%21RIV09-GA0-14310___
rdf:type
n16:Vysledek skos:Concept
dcterms:description
Structure analysis of [(C2H5)(n)(C6H5)(4-n)P](2)[TeBr6(Se2Br2)(2)] is presented for n=1 and 0 [ hereafter (I) and (II)]. Crystal (I) has been synthesized from elemental selenium, tellurium tetrabromide, ethyltriphenylphosphonium bromide and bromine. It has a standard monoclinic structure, space group P2(1)/c, and has been solved and refined to R=0.0357 for 4803 observed X-ray reflections by traditional techniques. Crystal (II), which has been prepared from elemental selenium, tellurium tetrabromide, tetraphenylphosphonium bromide and bromine, is an incommensurately one-dimensionally modulated structure with planar monoclinic superspace group. (II) has been refined to R=0.0501 for 4247 observed reflections. The modulation of the atoms that belong to the anion switches between two different basic positions, which are described by the crenel function algorithm. The modulation of the phenyl groups is much weaker and it could be refined within the rigid-body approximation. The TeBr6 octahedron is nearly re Structure analysis of [(C2H5)(n)(C6H5)(4-n)P](2)[TeBr6(Se2Br2)(2)] is presented for n=1 and 0 [ hereafter (I) and (II)]. Crystal (I) has been synthesized from elemental selenium, tellurium tetrabromide, ethyltriphenylphosphonium bromide and bromine. It has a standard monoclinic structure, space group P2(1)/c, and has been solved and refined to R=0.0357 for 4803 observed X-ray reflections by traditional techniques. Crystal (II), which has been prepared from elemental selenium, tellurium tetrabromide, tetraphenylphosphonium bromide and bromine, is an incommensurately one-dimensionally modulated structure with planar monoclinic superspace group. (II) has been refined to R=0.0501 for 4247 observed reflections. The modulation of the atoms that belong to the anion switches between two different basic positions, which are described by the crenel function algorithm. The modulation of the phenyl groups is much weaker and it could be refined within the rigid-body approximation. The TeBr6 octahedron is nearly re Structure analysis of [(C2H5)(n)(C6H5)(4-n)P](2)[TeBr6(Se2Br2)(2)] is presented for n=1 and 0 [ hereafter (I) and (II)]. Crystal (I) has been synthesized from elemental selenium, tellurium tetrabromide, ethyltriphenylphosphonium bromide and bromine. It has a standard monoclinic structure, space group P2(1)/c, and has been solved and refined to R=0.0357 for 4803 observed X-ray reflections by traditional techniques. Crystal (II), which has been prepared from elemental selenium, tellurium tetrabromide, tetraphenylphosphonium bromide and bromine, is an incommensurately one-dimensionally modulated structure with planar monoclinic superspace group. (II) has been refined to R=0.0501 for 4247 observed reflections. The modulation of the atoms that belong to the anion switches between two different basic positions, which are described by the crenel function algorithm. The modulation of the phenyl groups is much weaker and it could be refined within the rigid-body approximation. The TeBr6 octahedron is nearly re
dcterms:title
Commensurate and incommensurate structures of the hexabromotellurate(IV) bis {dibromodiselenate(I)} ion - [(C2H5)(n)(C6H5)(4-n)P](2)[TeBr6(Se2Br2)(2)], n=0,1 Commensurate and incommensurate structures of the hexabromotellurate(IV) bis {dibromodiselenate(I)} ion - [(C2H5)(n)(C6H5)(4-n)P](2)[TeBr6(Se2Br2)(2)], n=0,1 Commensurate and incommensurate structures of the hexabromotellurate(IV) bis {dibromodiselenate(I)} ion - [(C2H5)(n)(C6H5)(4-n)P](2)[TeBr6(Se2Br2)(2)], n=0,1
skos:prefLabel
Commensurate and incommensurate structures of the hexabromotellurate(IV) bis {dibromodiselenate(I)} ion - [(C2H5)(n)(C6H5)(4-n)P](2)[TeBr6(Se2Br2)(2)], n=0,1 Commensurate and incommensurate structures of the hexabromotellurate(IV) bis {dibromodiselenate(I)} ion - [(C2H5)(n)(C6H5)(4-n)P](2)[TeBr6(Se2Br2)(2)], n=0,1 Commensurate and incommensurate structures of the hexabromotellurate(IV) bis {dibromodiselenate(I)} ion - [(C2H5)(n)(C6H5)(4-n)P](2)[TeBr6(Se2Br2)(2)], n=0,1
skos:notation
RIV/00216224:14310/02:00007288!RIV09-GA0-14310___
n3:aktivita
n7:Z n7:P
n3:aktivity
P(GA202/00/0645), P(GA203/97/0955), P(GA203/98/0676), P(GA203/99/0067), Z(MSM 143100011)
n3:cisloPeriodika
6
n3:dodaniDat
n18:2009
n3:domaciTvurceVysledku
n8:1424343 n8:4027418
n3:druhVysledku
n12:J
n3:duvernostUdaju
n4:S
n3:entitaPredkladatele
n15:predkladatel
n3:idSjednocenehoVysledku
641200
n3:idVysledku
RIV/00216224:14310/02:00007288
n3:jazykVysledku
n13:eng
n3:klicovaSlova
CRYSTAL-STRUCTURES; SALTS
n3:klicoveSlovo
n5:SALTS n5:CRYSTAL-STRUCTURES
n3:kodStatuVydavatele
DK - Dánské království
n3:kontrolniKodProRIV
[828185A5BB2A]
n3:nazevZdroje
Acta Crystallographica Section B-Structural Science
n3:obor
n10:CA
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
5
n3:projekt
n9:GA203%2F99%2F0067 n9:GA203%2F97%2F0955 n9:GA202%2F00%2F0645 n9:GA203%2F98%2F0676
n3:rokUplatneniVysledku
n18:2002
n3:svazekPeriodika
58
n3:tvurceVysledku
Novosad, Josef Dušek, Michal Janickis, Vitalijus Nečas, Marek Petříček, Václav
n3:wos
000179551200009
n3:zamer
n17:MSM%20143100011
s:issn
0108-7681
s:numberOfPages
9
n11:organizacniJednotka
14310