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Statements

Subject Item
n2:RIV%2F00216208%3A11310%2F14%3A10282027%21RIV15-MSM-11310___
rdf:type
n4:Vysledek skos:Concept
rdfs:seeAlso
http://dx.doi.org/10.1016/j.electacta.2014.01.081
dcterms:description
This work demonstrates the applicability of differential pulse voltammetry (DPV) for the determination of the insecticide thiamethoxam at a non-toxic mercury meniscus modified silver solid amalgam electrode (m-AgSAE). The optimum supporting electrolyte was found to be Britton-Robinson (BR) buffer, pH 10. The target compound was quantified directly in spiked drinking and river water samples in the range from 100 mu mol L-1 to limits of determination (LOQs) 0.36 and 0.46 mu mol L-1, respectively. After preliminary separation and preconcentration by solid phase extraction (SPE) using Lichrolut EN cartridges, quantification in spiked river and drinking water samples was possible in the range from 100 nmol L-1 to LOQs 1.3 and 1.1 nmol L-1, respectively. m-AgSAE is practically non-toxic, possesses good mechanical stability and is easy to handle and activate and thus represents a suitable alternative to the hanging mercury drop electrode (HMDE). This work demonstrates the applicability of differential pulse voltammetry (DPV) for the determination of the insecticide thiamethoxam at a non-toxic mercury meniscus modified silver solid amalgam electrode (m-AgSAE). The optimum supporting electrolyte was found to be Britton-Robinson (BR) buffer, pH 10. The target compound was quantified directly in spiked drinking and river water samples in the range from 100 mu mol L-1 to limits of determination (LOQs) 0.36 and 0.46 mu mol L-1, respectively. After preliminary separation and preconcentration by solid phase extraction (SPE) using Lichrolut EN cartridges, quantification in spiked river and drinking water samples was possible in the range from 100 nmol L-1 to LOQs 1.3 and 1.1 nmol L-1, respectively. m-AgSAE is practically non-toxic, possesses good mechanical stability and is easy to handle and activate and thus represents a suitable alternative to the hanging mercury drop electrode (HMDE).
dcterms:title
Voltammetric Determination of Insecticide Thiamethoxam on Silver Solid Amalgam Electrode Voltammetric Determination of Insecticide Thiamethoxam on Silver Solid Amalgam Electrode
skos:prefLabel
Voltammetric Determination of Insecticide Thiamethoxam on Silver Solid Amalgam Electrode Voltammetric Determination of Insecticide Thiamethoxam on Silver Solid Amalgam Electrode
skos:notation
RIV/00216208:11310/14:10282027!RIV15-MSM-11310___
n5:aktivita
n19:I n19:P
n5:aktivity
I, P(7AMB12GR003), P(GBP206/12/G151)
n5:cisloPeriodika
September
n5:dodaniDat
n10:2015
n5:domaciTvurceVysledku
n7:1874098 n7:4454472 Chorti, Parthena n7:8805865
n5:druhVysledku
n18:J
n5:duvernostUdaju
n17:S
n5:entitaPredkladatele
n8:predkladatel
n5:idSjednocenehoVysledku
54151
n5:idVysledku
RIV/00216208:11310/14:10282027
n5:jazykVysledku
n20:eng
n5:klicovaSlova
River water; Drinking water; Solid phase extraction; Silver solid amalgam electrode; Differential pulse voltammetry (DPV); Thiamethoxam
n5:klicoveSlovo
n12:Solid%20phase%20extraction n12:Thiamethoxam n12:Silver%20solid%20amalgam%20electrode n12:Drinking%20water n12:River%20water n12:Differential%20pulse%20voltammetry%20%28DPV%29
n5:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n5:kontrolniKodProRIV
[49E380AC0206]
n5:nazevZdroje
Electrochimica Acta
n5:obor
n14:CG
n5:pocetDomacichTvurcuVysledku
4
n5:pocetTvurcuVysledku
5
n5:projekt
n9:GBP206%2F12%2FG151 n9:7AMB12GR003
n5:rokUplatneniVysledku
n10:2014
n5:svazekPeriodika
140
n5:tvurceVysledku
Economou, Anastasios Fischer, Jan Chorti, Parthena Barek, Jiří Vyskočil, Vlastimil
n5:wos
000342528600002
s:issn
0013-4686
s:numberOfPages
6
n16:doi
10.1016/j.electacta.2014.01.081
n15:organizacniJednotka
11310