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Statements

Subject Item
n2:RIV%2F00216208%3A11310%2F13%3A10139695%21RIV14-MSM-11310___
rdf:type
n9:Vysledek skos:Concept
rdfs:seeAlso
http://www.sciencedirect.com/science/article/pii/S0026265X12001415
dcterms:description
A new combination of flow-through electrochemical mercury cold vapor generation using a microstrip microwave plasma optical emission spectrometry is described in thiswork. This coupled technique has been optimized to attain the maximum sensitivity for Hg determinations in aqueous solutions and the lower limits of detection. A laboratory constructed thin-layer flow-through hydrogen remover (inner volume of 2x150 μL) was used. A limit of detection of 1.1 ng.mLMINUS SIGN 1 (peak height, 3σ criterion) for mercury was obtained with the proposed method when using electrochemical mercury cold vapor generation. Further, the results obtained with spiked SRM NIST 1640 and SRM NIST 2781 were verified by ICP-OES and a good agreement at the concentration levels of 2.72+-0.37 μg.gMINUS SIGN 1 and 2.80+-0.25 μg.gMINUS SIGN 1 was obtained. The repeatability at the 50 ng.mLMINUS SIGN 1 level was better than 2.7% (RSD). A new combination of flow-through electrochemical mercury cold vapor generation using a microstrip microwave plasma optical emission spectrometry is described in thiswork. This coupled technique has been optimized to attain the maximum sensitivity for Hg determinations in aqueous solutions and the lower limits of detection. A laboratory constructed thin-layer flow-through hydrogen remover (inner volume of 2x150 μL) was used. A limit of detection of 1.1 ng.mLMINUS SIGN 1 (peak height, 3σ criterion) for mercury was obtained with the proposed method when using electrochemical mercury cold vapor generation. Further, the results obtained with spiked SRM NIST 1640 and SRM NIST 2781 were verified by ICP-OES and a good agreement at the concentration levels of 2.72+-0.37 μg.gMINUS SIGN 1 and 2.80+-0.25 μg.gMINUS SIGN 1 was obtained. The repeatability at the 50 ng.mLMINUS SIGN 1 level was better than 2.7% (RSD).
dcterms:title
Determination of mercury in water samples by electrochemical cold vapor generation coupled to microstrip microwave induced helium plasma optical emission spectrometry Determination of mercury in water samples by electrochemical cold vapor generation coupled to microstrip microwave induced helium plasma optical emission spectrometry
skos:prefLabel
Determination of mercury in water samples by electrochemical cold vapor generation coupled to microstrip microwave induced helium plasma optical emission spectrometry Determination of mercury in water samples by electrochemical cold vapor generation coupled to microstrip microwave induced helium plasma optical emission spectrometry
skos:notation
RIV/00216208:11310/13:10139695!RIV14-MSM-11310___
n9:predkladatel
n10:orjk%3A11310
n3:aktivita
n12:I n12:P n12:Z
n3:aktivity
I, P(IAA400310507), Z(MSM0021620857)
n3:cisloPeriodika
march 2013
n3:dodaniDat
n7:2014
n3:domaciTvurceVysledku
n13:2509083
n3:druhVysledku
n11:J
n3:duvernostUdaju
n17:S
n3:entitaPredkladatele
n18:predkladatel
n3:idSjednocenehoVysledku
68892
n3:idVysledku
RIV/00216208:11310/13:10139695
n3:jazykVysledku
n8:eng
n3:klicovaSlova
Optical emission spectrometry; Mercury determination; Microstrip microwave induced plasma; Electrochemical cold vapor generation
n3:klicoveSlovo
n15:Mercury%20determination n15:Optical%20emission%20spectrometry n15:Electrochemical%20cold%20vapor%20generation n15:Microstrip%20microwave%20induced%20plasma
n3:kodStatuVydavatele
NL - Nizozemsko
n3:kontrolniKodProRIV
[D64E1702233C]
n3:nazevZdroje
Microchemical Journal
n3:obor
n5:CB
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
3
n3:projekt
n22:IAA400310507
n3:rokUplatneniVysledku
n7:2013
n3:svazekPeriodika
107
n3:tvurceVysledku
Horváth, Márk Broekaert, José Alfons Clement Červený, Václav
n3:wos
000315059500003
n3:zamer
n19:MSM0021620857
s:issn
0026-265X
s:numberOfPages
7
n16:doi
10.1016/j.microc.2012.05.023
n20:organizacniJednotka
11310