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Statements

Subject Item
n2:RIV%2F00216208%3A11310%2F11%3A10105663%21RIV12-TA0-11310___
rdf:type
skos:Concept n13:Vysledek
rdfs:seeAlso
http://dx.doi.org/10.1135/cccc2011142
dcterms:description
Electrochemical behavior of genotoxic 2-aminofluoren-9-one (2-AFN) was investigated by DC tast polarography (DCTP) and differential pulse polarography (DPP), both at a classical dropping mercury electrode (DME), and by DC voltammetry (DCV), differential pulse voltammetry (DPV), and adsorptive stripping differential pulse voltammetry (AdSDPV), all at a miniaturized hanging mercury drop minielectrode (HMDmE), in buffered aqueous-methanolic solutions. Optimum conditions were found for the determination of 2-AFN by DCTP at DME in the concentration range from 1 x 10-6 to 1 x 10-4 mol l-1 (with a limit of quantification (LQ) of 5 x 10-7 mol l-1), by DPP at DME (from 1 x 10-7 to 1 x 10-4 mol l-1; LQ on level of 1 x 10-7 mol l-1), by DCV and DPV at HMDmE (both from 1 x 10-7 to 1 x 10-4 mol l-1; LQs on level of 2 x 10-7 and 1 x 10-7 mol l-1 for DCV and DPV, respectively), and by AdSDPV at HMDmE (from 2 x 10-9 to 1 x 10-7 mol l-1; LQ ALMOST EQUAL TO 4 x 10-9 mol l-1). Practical applicability of the developed methods was verified on the direct determination of 2-AFN in model samples of drinking and river water in nanomolar to micromolar concentrations. Electrochemical behavior of genotoxic 2-aminofluoren-9-one (2-AFN) was investigated by DC tast polarography (DCTP) and differential pulse polarography (DPP), both at a classical dropping mercury electrode (DME), and by DC voltammetry (DCV), differential pulse voltammetry (DPV), and adsorptive stripping differential pulse voltammetry (AdSDPV), all at a miniaturized hanging mercury drop minielectrode (HMDmE), in buffered aqueous-methanolic solutions. Optimum conditions were found for the determination of 2-AFN by DCTP at DME in the concentration range from 1 x 10-6 to 1 x 10-4 mol l-1 (with a limit of quantification (LQ) of 5 x 10-7 mol l-1), by DPP at DME (from 1 x 10-7 to 1 x 10-4 mol l-1; LQ on level of 1 x 10-7 mol l-1), by DCV and DPV at HMDmE (both from 1 x 10-7 to 1 x 10-4 mol l-1; LQs on level of 2 x 10-7 and 1 x 10-7 mol l-1 for DCV and DPV, respectively), and by AdSDPV at HMDmE (from 2 x 10-9 to 1 x 10-7 mol l-1; LQ ALMOST EQUAL TO 4 x 10-9 mol l-1). Practical applicability of the developed methods was verified on the direct determination of 2-AFN in model samples of drinking and river water in nanomolar to micromolar concentrations.
dcterms:title
Polarographic and voltammetric determination of genotoxic 2-aminofluoren-9-one at mercury electrodes Polarographic and voltammetric determination of genotoxic 2-aminofluoren-9-one at mercury electrodes
skos:prefLabel
Polarographic and voltammetric determination of genotoxic 2-aminofluoren-9-one at mercury electrodes Polarographic and voltammetric determination of genotoxic 2-aminofluoren-9-one at mercury electrodes
skos:notation
RIV/00216208:11310/11:10105663!RIV12-TA0-11310___
n13:predkladatel
n14:orjk%3A11310
n3:aktivita
n8:Z n8:S n8:P
n3:aktivity
P(LC06035), P(ME10004), P(TA01020565), S, Z(MSM0021620857)
n3:cisloPeriodika
12
n3:dodaniDat
n6:2012
n3:domaciTvurceVysledku
n11:4454472 n11:3609634 n11:2674076 n11:8805865
n3:druhVysledku
n17:J
n3:duvernostUdaju
n22:S
n3:entitaPredkladatele
n4:predkladatel
n3:idSjednocenehoVysledku
221068
n3:idVysledku
RIV/00216208:11310/11:10105663
n3:jazykVysledku
n18:eng
n3:klicovaSlova
Spiked water samples; 2-Aminofluoren-9-one; Mercury electrodes; Voltammetry; Polarography; Electrochemistry; Analytical methods
n3:klicoveSlovo
n9:2-Aminofluoren-9-one n9:Mercury%20electrodes n9:Analytical%20methods n9:Electrochemistry n9:Polarography n9:Voltammetry n9:Spiked%20water%20samples
n3:kodStatuVydavatele
CZ - Česká republika
n3:kontrolniKodProRIV
[9FFC65F85C51]
n3:nazevZdroje
Collection of Czechoslovak Chemical Communications
n3:obor
n5:CG
n3:pocetDomacichTvurcuVysledku
4
n3:pocetTvurcuVysledku
5
n3:projekt
n10:TA01020565 n10:ME10004 n10:LC06035
n3:rokUplatneniVysledku
n6:2011
n3:svazekPeriodika
76
n3:tvurceVysledku
Vyskočil, Vlastimil Barek, Jiří Hájková, Andrea Wang, Joseph Daňhel, Aleš
n3:wos
000299816100023
n3:zamer
n21:MSM0021620857
s:issn
0010-0765
s:numberOfPages
13
n20:doi
10.1135/cccc2011142
n19:organizacniJednotka
11310