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Statements

Subject Item
n2:RIV%2F00216208%3A11310%2F10%3A10061943%21RIV11-MSM-11310___
rdf:type
n7:Vysledek skos:Concept
dcterms:description
The study compares HPLC determination of 2-aminobiphenyl, 3-aminobiphenyl, and 4-aminobiphenyl using amperometric detection at a microcrystalline boron-doped diamond film electrode in thin-layer and wall-jet arrangement. Satisfactory separation of studied analytes was achieved at a ChiraDex column (Merck) with chemically bonded beta-cyclodextrin in mobile phase consisting of 0.01 mol L-1 acetate buffer, pH 5 : acetonitrile : methanol (40:30:30; v/v/v) with total analysis time of six minutes. The repeatabilities of the detector responses are satisfactory. Slightly wider linear dynamic range of calibration dependencies and lower detection limits in the 10-8 mol L-1 concentration range were achieved for the walljet arrangement. The study compares HPLC determination of 2-aminobiphenyl, 3-aminobiphenyl, and 4-aminobiphenyl using amperometric detection at a microcrystalline boron-doped diamond film electrode in thin-layer and wall-jet arrangement. Satisfactory separation of studied analytes was achieved at a ChiraDex column (Merck) with chemically bonded beta-cyclodextrin in mobile phase consisting of 0.01 mol L-1 acetate buffer, pH 5 : acetonitrile : methanol (40:30:30; v/v/v) with total analysis time of six minutes. The repeatabilities of the detector responses are satisfactory. Slightly wider linear dynamic range of calibration dependencies and lower detection limits in the 10-8 mol L-1 concentration range were achieved for the walljet arrangement.
dcterms:title
Amperometric detection of aminobiphenyls in HPLC using microcrystalline boron- doped diamond Film Electrode in %22Wall-Jet%22 and %22Thin-Layer%22 arrangement Amperometric detection of aminobiphenyls in HPLC using microcrystalline boron- doped diamond Film Electrode in %22Wall-Jet%22 and %22Thin-Layer%22 arrangement
skos:prefLabel
Amperometric detection of aminobiphenyls in HPLC using microcrystalline boron- doped diamond Film Electrode in %22Wall-Jet%22 and %22Thin-Layer%22 arrangement Amperometric detection of aminobiphenyls in HPLC using microcrystalline boron- doped diamond Film Electrode in %22Wall-Jet%22 and %22Thin-Layer%22 arrangement
skos:notation
RIV/00216208:11310/10:10061943!RIV11-MSM-11310___
n3:aktivita
n5:S n5:P n5:V n5:Z
n3:aktivity
P(LC06035), S, V, Z(MSM0021620857)
n3:dodaniDat
n16:2011
n3:domaciTvurceVysledku
n4:1623532 n4:4454472 n4:3329194
n3:druhVysledku
n11:D
n3:duvernostUdaju
n19:S
n3:entitaPredkladatele
n15:predkladatel
n3:idSjednocenehoVysledku
246121
n3:idVysledku
RIV/00216208:11310/10:10061943
n3:jazykVysledku
n12:eng
n3:klicovaSlova
aminobiphenyls; wall-jet arrangement; thinlayer arrangement; amperometric detection; HPLC; boron-doped diamond film electrode
n3:klicoveSlovo
n6:wall-jet%20arrangement n6:amperometric%20detection n6:thinlayer%20arrangement n6:HPLC n6:boron-doped%20diamond%20film%20electrode n6:aminobiphenyls
n3:kontrolniKodProRIV
[184B215E13E4]
n3:mistoKonaniAkce
Jetřichovice
n3:mistoVydani
Ústí nad Labem
n3:nazevZdroje
Sborník přednášek mezinárodní odborné konference XXX. Moderní Elektrochemické Metody, Jetřichovice 24. ? 28. května 2010
n3:obor
n18:CG
n3:pocetDomacichTvurcuVysledku
3
n3:pocetTvurcuVysledku
3
n3:projekt
n20:LC06035
n3:rokUplatneniVysledku
n16:2010
n3:tvurceVysledku
Pecková, Karolina Barek, Jiří Maixnerová, Lucie
n3:typAkce
n14:EUR
n3:wos
000283050900024
n3:zahajeniAkce
2010-05-24+02:00
n3:zamer
n21:MSM0021620857
s:numberOfPages
5
n17:hasPublisher
Best servis Ústí nad Labem
n13:isbn
978-80-254-6710-7
n22:organizacniJednotka
11310