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Statements

Subject Item
n2:RIV%2F00216208%3A11310%2F10%3A10056957%21RIV11-MSM-11310___
rdf:type
n10:Vysledek skos:Concept
dcterms:description
RP-HPLC and non-aqueous CZE methods were evaluated for qualitative and quantitative analysis of esterified macrocyclic compounds of the DOTA family (DOTA = 1,4,7,10-tetraazacyclododecan-1,4,7,10-tetraacetic: acid). This group of compounds represents important reaction intermediates in synthesis of magnetic resonance contrast agents. Calibration curves in the concentration range from 1.0 x 10(-5) to 1.0 x 10(-3) mol/L were plotted and the experimental data were critically compared in terms of their repeatability, linearity, LOD and LOQ. The optimized methods were successfully applied to the analysis of a real reaction mixture without any further pretreatment. RP-HPLC and non-aqueous CZE methods were evaluated for qualitative and quantitative analysis of esterified macrocyclic compounds of the DOTA family (DOTA = 1,4,7,10-tetraazacyclododecan-1,4,7,10-tetraacetic: acid). This group of compounds represents important reaction intermediates in synthesis of magnetic resonance contrast agents. Calibration curves in the concentration range from 1.0 x 10(-5) to 1.0 x 10(-3) mol/L were plotted and the experimental data were critically compared in terms of their repeatability, linearity, LOD and LOQ. The optimized methods were successfully applied to the analysis of a real reaction mixture without any further pretreatment.
dcterms:title
Comparison of HPLC and CZE methods for analysis of DOTA-like esters - reaction intermediates in synthesis of magnetic resonance contrast agents Comparison of HPLC and CZE methods for analysis of DOTA-like esters - reaction intermediates in synthesis of magnetic resonance contrast agents
skos:prefLabel
Comparison of HPLC and CZE methods for analysis of DOTA-like esters - reaction intermediates in synthesis of magnetic resonance contrast agents Comparison of HPLC and CZE methods for analysis of DOTA-like esters - reaction intermediates in synthesis of magnetic resonance contrast agents
skos:notation
RIV/00216208:11310/10:10056957!RIV11-MSM-11310___
n3:aktivita
n6:Z n6:S
n3:aktivity
S, Z(MSM0021620857)
n3:cisloPeriodika
4-5
n3:dodaniDat
n17:2011
n3:domaciTvurceVysledku
n5:6532667 n5:9695656 n5:1015133 n5:4722744 n5:9174400
n3:druhVysledku
n12:J
n3:duvernostUdaju
n18:S
n3:entitaPredkladatele
n11:predkladatel
n3:idSjednocenehoVysledku
251448
n3:idVysledku
RIV/00216208:11310/10:10056957
n3:jazykVysledku
n14:eng
n3:klicovaSlova
acid; plasma; instrumentation; lanthanide complexes; liquid-chromatographic determination
n3:klicoveSlovo
n9:lanthanide%20complexes n9:instrumentation n9:acid n9:plasma n9:liquid-chromatographic%20determination
n3:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n3:kontrolniKodProRIV
[04A91DFF990F]
n3:nazevZdroje
Journal of Separation Science
n3:obor
n16:CB
n3:pocetDomacichTvurcuVysledku
5
n3:pocetTvurcuVysledku
5
n3:rokUplatneniVysledku
n17:2010
n3:svazekPeriodika
33
n3:tvurceVysledku
Coufal, Pavel Křížek, Tomáš Kubíček, Vojtěch Bosáková, Zuzana Hamplová, Anna
n3:wos
000276573800027
n3:zamer
n7:MSM0021620857
s:issn
1615-9306
s:numberOfPages
6
n15:organizacniJednotka
11310