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Statements

Subject Item
n2:RIV%2F00216208%3A11310%2F09%3A10001002%21RIV10-MSM-11310___
rdf:type
n4:Vysledek skos:Concept
dcterms:description
Thermolysis of [TiMe2(eta(5)-C5Me4Ph)(2)] (4) at 145 degrees C for 5 h afforded the singly tucked-in paramagnetictitanocene [Ti(III)(eta(5)-C5Me4Ph){eta(5):eta(1)-C5Me3Ph(CH2)}] (9). In distinction to the singly tucked-in permethyltitanocene [Ti(III)(eta(5)-C5Me5)(eta(5):eta(1)-C5Me4(CH2))] (1) which was found crystallographically disordered [J.M. Fischer, W.E. Piers, V.G. Young, Jr., Organometallics 15 (1996) 2410] the single crystal X-ray diffraction analysis of 9 afforded molecular parameters with nearly by one order better precision as measured by esd-values. Thermolysis of [TiMe2(eta(5)-C5Me4Ph)(2)] (4) at 145 degrees C for 5 h afforded the singly tucked-in paramagnetictitanocene [Ti(III)(eta(5)-C5Me4Ph){eta(5):eta(1)-C5Me3Ph(CH2)}] (9). In distinction to the singly tucked-in permethyltitanocene [Ti(III)(eta(5)-C5Me5)(eta(5):eta(1)-C5Me4(CH2))] (1) which was found crystallographically disordered [J.M. Fischer, W.E. Piers, V.G. Young, Jr., Organometallics 15 (1996) 2410] the single crystal X-ray diffraction analysis of 9 afforded molecular parameters with nearly by one order better precision as measured by esd-values.
dcterms:title
Synthesis and crystal structure of the singly tucked-in derivative of bis(phenyltetramethylcyclopentadienyl)titanium Synthesis and crystal structure of the singly tucked-in derivative of bis(phenyltetramethylcyclopentadienyl)titanium
skos:prefLabel
Synthesis and crystal structure of the singly tucked-in derivative of bis(phenyltetramethylcyclopentadienyl)titanium Synthesis and crystal structure of the singly tucked-in derivative of bis(phenyltetramethylcyclopentadienyl)titanium
skos:notation
RIV/00216208:11310/09:10001002!RIV10-MSM-11310___
n3:aktivita
n7:Z n7:P
n3:aktivity
P(IAA400400708), P(LC06070), P(LC06071), Z(AV0Z40400503)
n3:cisloPeriodika
1
n3:dodaniDat
n12:2010
n3:domaciTvurceVysledku
n11:3157962
n3:druhVysledku
n8:J
n3:duvernostUdaju
n6:S
n3:entitaPredkladatele
n15:predkladatel
n3:idSjednocenehoVysledku
345069
n3:idVysledku
RIV/00216208:11310/09:10001002
n3:jazykVysledku
n18:eng
n3:klicovaSlova
titanium; titanocene; tucked-in
n3:klicoveSlovo
n14:tucked-in n14:titanium n14:titanocene
n3:kodStatuVydavatele
NL - Nizozemsko
n3:kontrolniKodProRIV
[CE9F7527A0D1]
n3:nazevZdroje
Inorganic Chemistry Communications
n3:obor
n19:CF
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
7
n3:projekt
n9:LC06071 n9:LC06070 n9:IAA400400708
n3:rokUplatneniVysledku
n12:2009
n3:svazekPeriodika
12
n3:tvurceVysledku
Conde, A. Císařová, Ivana Kubišta, Jiří Horáček, Michal Fandos, R. Pinkas, Jiří Mach, Karel
n3:wos
000262891400004
n3:zamer
n16:AV0Z40400503
s:issn
1387-7003
s:numberOfPages
4
n17:organizacniJednotka
11310