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Statements

Subject Item
n2:RIV%2F00025798%3A_____%2F14%3A00000113%21RIV15-MSM-00025798
rdf:type
skos:Concept n18:Vysledek
rdfs:seeAlso
http://pubs.rsc.org/en/Content/ArticleLanding/2014/JA/c3ja50241d#!divAbstract
dcterms:description
Laser ablation multi-collector inductively coupled plasma mass spectrometry (LA MC ICP-MS) and secondary ion mass spectrometry (SIMS) were used to determine the boron isotopic compositions of several natural tourmaline group minerals (elbaite, schorl and dravite). This study reports on the effects of instrument parameters of LA MC ICP-MS and the composition of sample matrix on data accuracy, reproducibility and repeatability. We demonstrate that the tourmaline matrix has a significant effect on the obtained delta B-11 values and impacts on data accuracy, with a bias of up to ca. 2.5 parts per thousand if a non matrix-matched reference material is used to calibrate the measurements. In the case of a matrix-matched calibration, the boron isotopic data obtained by LA MC ICP-MS are comparable to the reference TIMS values, with typical repeatability for delta B-11 results between 0.2 and 0.5 parts per thousand (1s). This is somewhat better compared to the repeatability of 0.8-1.3 parts per thousand (1s) for small format single collector SIMS. Laser ablation multi-collector inductively coupled plasma mass spectrometry (LA MC ICP-MS) and secondary ion mass spectrometry (SIMS) were used to determine the boron isotopic compositions of several natural tourmaline group minerals (elbaite, schorl and dravite). This study reports on the effects of instrument parameters of LA MC ICP-MS and the composition of sample matrix on data accuracy, reproducibility and repeatability. We demonstrate that the tourmaline matrix has a significant effect on the obtained delta B-11 values and impacts on data accuracy, with a bias of up to ca. 2.5 parts per thousand if a non matrix-matched reference material is used to calibrate the measurements. In the case of a matrix-matched calibration, the boron isotopic data obtained by LA MC ICP-MS are comparable to the reference TIMS values, with typical repeatability for delta B-11 results between 0.2 and 0.5 parts per thousand (1s). This is somewhat better compared to the repeatability of 0.8-1.3 parts per thousand (1s) for small format single collector SIMS.
dcterms:title
Matrix effects during laser ablation MC ICP-MS analysis of boron isotopes in tourmaline Matrix effects during laser ablation MC ICP-MS analysis of boron isotopes in tourmaline
skos:prefLabel
Matrix effects during laser ablation MC ICP-MS analysis of boron isotopes in tourmaline Matrix effects during laser ablation MC ICP-MS analysis of boron isotopes in tourmaline
skos:notation
RIV/00025798:_____/14:00000113!RIV15-MSM-00025798
n3:aktivita
n8:I
n3:aktivity
I
n3:cisloPeriodika
5
n3:dodaniDat
n7:2015
n3:domaciTvurceVysledku
n11:7404352
n3:druhVysledku
n9:J
n3:duvernostUdaju
n12:S
n3:entitaPredkladatele
n16:predkladatel
n3:idSjednocenehoVysledku
27679
n3:idVysledku
RIV/00025798:_____/14:00000113
n3:jazykVysledku
n17:eng
n3:klicovaSlova
Plasma-mass spectrometry, Laser ablation, Secondary ion mass spectrometry, Martix effects, Boron isotopes, Elemental fractionation, Mannitol complex, Ion microprobe, Geochemistry
n3:klicoveSlovo
n4:Secondary%20ion%20mass%20spectrometry n4:Geochemistry n4:Laser%20ablation n4:Ion%20microprobe n4:Boron%20isotopes n4:Martix%20effects n4:Elemental%20fractionation n4:Mannitol%20complex n4:Plasma-mass%20spectrometry
n3:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n3:kontrolniKodProRIV
[DF4846C4C185]
n3:nazevZdroje
Journal of Analytical Atomic Spectrometry
n3:obor
n5:CB
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
3
n3:rokUplatneniVysledku
n7:2014
n3:svazekPeriodika
29
n3:tvurceVysledku
Míková, Jitka Wiedenbeck, Michael Košler, Jan
n3:wos
000334737300014
s:issn
0267-9477
s:numberOfPages
12
n13:doi
10.1039/c3ja50241d