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  • In the present work, we report on successful preparation of twinned hexagonal ZnO microparticles in modified domestic microwave oven using zinc acetate dehydrate and hexamethylenetetramine. While no surfactants or capping agents were used, fully developed twinned hexagonal microparticles were synthesized in 7 minutes. The morphology was studied by scanning electron microscopy and the crystal phase structure was verified by X-ray diffractometry. Short synthesis time, high reproducibility and environment benign starting chemicals make this method suitable candidate for large-scale production.
  • In the present work, we report on successful preparation of twinned hexagonal ZnO microparticles in modified domestic microwave oven using zinc acetate dehydrate and hexamethylenetetramine. While no surfactants or capping agents were used, fully developed twinned hexagonal microparticles were synthesized in 7 minutes. The morphology was studied by scanning electron microscopy and the crystal phase structure was verified by X-ray diffractometry. Short synthesis time, high reproducibility and environment benign starting chemicals make this method suitable candidate for large-scale production. (en)
Title
  • Rapid Microwave-assisted Synthesis of Twinned Hexagonal ZnO Microparticles
  • Rapid Microwave-assisted Synthesis of Twinned Hexagonal ZnO Microparticles (en)
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  • Rapid Microwave-assisted Synthesis of Twinned Hexagonal ZnO Microparticles
  • Rapid Microwave-assisted Synthesis of Twinned Hexagonal ZnO Microparticles (en)
skos:notation
  • RIV/70883521:28610/11:43867122!RIV12-MSM-28610___
http://linked.open...avai/predkladatel
http://linked.open...avai/riv/aktivita
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  • P(ED2.1.00/03.0111), Z(MSM7088352101)
http://linked.open...vai/riv/dodaniDat
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  • 225709
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  • RIV/70883521:28610/11:43867122
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  • ZnO, Microwave synthesis (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...ontrolniKodProRIV
  • [864510131B9D]
http://linked.open...v/mistoKonaniAkce
  • Catania
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  • Venice
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  • Mathematical Methods and Techniques in Engineering and Environmental Science
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  • Kuřitka, Ivo
  • Machovský, Michal
  • Sáha, Petr
http://linked.open...vavai/riv/typAkce
http://linked.open.../riv/zahajeniAkce
http://linked.open...n/vavai/riv/zamer
number of pages
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  • WSEAS Press (IT)
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  • 978-1-61804-046-6
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  • 28610
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