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  • A modified semimicro method is described for determining chemical oxygen demand (COD) employing microwave (MW) digestion (0.5 min exposure at 1,000 W power, and 10 min exposure at 250 W power) with a titration assessment. Composition of reaction mixture was the same as that of the usual reflux method. Determfination was performed in glass vessels of original tetrafluoromethoxil containers. Under given conditions dichromate autoreduction was low. A good agreement with the usual reflux method was obtainedwith selected substances (potassium hydrogen phthalate, glutamic acid, glucose, dodecyl sulphate, where COD-MW/ThOD is 98.9 - 101.5 %). With real samples (municipal sewage, mixed tanning and chemical wastewaters, and treated wastewater from biological t reatment plants) the obtained results were also satisfactory (88.0 - 111.9 %)
  • A modified semimicro method is described for determining chemical oxygen demand (COD) employing microwave (MW) digestion (0.5 min exposure at 1,000 W power, and 10 min exposure at 250 W power) with a titration assessment. Composition of reaction mixture was the same as that of the usual reflux method. Determfination was performed in glass vessels of original tetrafluoromethoxil containers. Under given conditions dichromate autoreduction was low. A good agreement with the usual reflux method was obtainedwith selected substances (potassium hydrogen phthalate, glutamic acid, glucose, dodecyl sulphate, where COD-MW/ThOD is 98.9 - 101.5 %). With real samples (municipal sewage, mixed tanning and chemical wastewaters, and treated wastewater from biological t reatment plants) the obtained results were also satisfactory (88.0 - 111.9 %) (en)
Title
  • Semimicro Determination of COD Employing Microwave Digestion
  • Semimicro Determination of COD Employing Microwave Digestion (en)
skos:prefLabel
  • Semimicro Determination of COD Employing Microwave Digestion
  • Semimicro Determination of COD Employing Microwave Digestion (en)
skos:notation
  • RIV/70883521:28110/03:63501396!RIV/2004/MSM/281104/N
http://linked.open.../vavai/riv/strany
  • 617-626
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM 281100002)
http://linked.open...iv/cisloPeriodika
  • 6
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 626685
http://linked.open...ai/riv/idVysledku
  • RIV/70883521:28110/03:63501396
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • chemical oxygen demand, COD, microwave digestion, MW, COD-MW, Cr, Hg, Ag (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • US - Spojené státy americké
http://linked.open...ontrolniKodProRIV
  • [C9AD76933C55]
http://linked.open...i/riv/nazevZdroje
  • Environmental Engineering Science
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...ocetUcastnikuAkce
http://linked.open...nichUcastnikuAkce
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 20
http://linked.open...iv/tvurceVysledku
  • Houser, Josef
http://linked.open...n/vavai/riv/zamer
issn
  • 1092-8758
number of pages
http://localhost/t...ganizacniJednotka
  • 28110
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