About: The Synthesis of N-derivatives of 3-Aminoperylene and their Absorption and Fluorescence Properties

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About: The Synthesis of N-derivatives of 3-Aminoperylene and their Absorption and Fluorescence Properties Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	N-acetyl and N-triazinyl 3-aminoperylenes were prepared. N-(4,6-dichloro-1,3,5-triazine-2-yl)-3-aminoperylene was synthesized by the condensation of 3-aminoperylene with cyanuric chloride; other N-triazinyl derivatives were prepared by the successive substitution of chlorine atoms with methoxy or aniline groups. The structure and purity of the compounds were confirmed by elemental analysis, NMR spectroscopy and mass spectrometry. The UV/VIS absorption, fluorescence and excitation spectra as well as the fluorescence quantum yields for the compounds were measured in dibutyl ether, 1,4-dioxane, ethyl acetate and acetonitrile; fluorescence lifetimes were measured in ethyl acetate and dimethyl sulfoxide. The influences of both the character of the N-substituent and the solvent polarity upon the spectra and quantum yields are discussed. N-acetyl and N-triazinyl 3-aminoperylenes were prepared. N-(4,6-dichloro-1,3,5-triazine-2-yl)-3-aminoperylene was synthesized by the condensation of 3-aminoperylene with cyanuric chloride; other N-triazinyl derivatives were prepared by the successive substitution of chlorine atoms with methoxy or aniline groups. The structure and purity of the compounds were confirmed by elemental analysis, NMR spectroscopy and mass spectrometry. The UV/VIS absorption, fluorescence and excitation spectra as well as the fluorescence quantum yields for the compounds were measured in dibutyl ether, 1,4-dioxane, ethyl acetate and acetonitrile; fluorescence lifetimes were measured in ethyl acetate and dimethyl sulfoxide. The influences of both the character of the N-substituent and the solvent polarity upon the spectra and quantum yields are discussed. (en)
Title	The Synthesis of N-derivatives of 3-Aminoperylene and their Absorption and Fluorescence Properties The Synthesis of N-derivatives of 3-Aminoperylene and their Absorption and Fluorescence Properties (en)
skos:prefLabel	The Synthesis of N-derivatives of 3-Aminoperylene and their Absorption and Fluorescence Properties The Synthesis of N-derivatives of 3-Aminoperylene and their Absorption and Fluorescence Properties (en)
skos:notation	RIV/68407700:21340/09:00160789!RIV14-MSM-21340___
http://linked.open...avai/riv/aktivita	S Z
http://linked.open...avai/riv/aktivity	S, Z(MSM0021627501)
http://linked.open...iv/cisloPeriodika	2
http://linked.open...vai/riv/dodaniDat	2014
http://linked.open...aciTvurceVysledku	Dvořák, Miroslav Michl, Martin
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	České vysoké učení technické v Praze / Fakulta jaderná a fyzikálně inženýrská
http://linked.open...dnocenehoVysledku	345111
http://linked.open...ai/riv/idVysledku	RIV/68407700:21340/09:00160789
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	3-Aminoperylene N-derivatives; Absorption; Fluorescence; Quantum yield (en)
http://linked.open.../riv/klicoveSlovo	Fluorescence 3-Aminoperylene N-derivatives Absorption Quantum yield
http://linked.open...odStatuVydavatele	NL - Nizozemsko
http://linked.open...ontrolniKodProRIV	[C8AA8766F152]
http://linked.open...i/riv/nazevZdroje	Dyes and Pigments
http://linked.open...in/vavai/riv/obor	CC
http://linked.open...ichTvurcuVysledku	2 (xsd:int)
http://linked.open...cetTvurcuVysledku	7 (xsd:int)
http://linked.open...UplatneniVysledku	2009
http://linked.open...v/svazekPeriodika	82
http://linked.open...iv/tvurceVysledku	Dvořák, Miroslav Almonasy, N. Michl, Martin Nepraš, Miloš Čermák, J. Lyčka, A. Hyková, Š.
http://linked.open...ain/vavai/riv/wos	000265520400011
http://linked.open...n/vavai/riv/zamer	Aimed preparation of special compounds and materials and investigation of their physical and chemical properties and supramolecular structures
issn	0143-7208
number of pages	7 (xsd:int)
http://bibframe.org/vocab/doi	10.1016/j.dyepig.2008.12.009
http://localhost/t...ganizacniJednotka	21340

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