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  • Several open questions related to the experimental protocol and processing of data acquired by the nano-indentation technique are investigated. The volume fractions of mechanically different phases obtained from statistical analysis are shown to be different from those obtained by back-scattered electron image analysis and X-ray diffraction method on the same paste. Judging from transmission electron microscope images, the representative volume element of low-density calcium-silicate hydrates can be considered to be around 500 nm, whereas for high-density C-S-H it is about 100 nm. This raises the question how the appropriate penetration depth for NI experiments should be selected. Changing the maximum load from 1 mN to 5 mN, the effect of penetration depth on the experimental results is studied. As an alternative, a %22manual%22 indentation method is proposed.
  • Several open questions related to the experimental protocol and processing of data acquired by the nano-indentation technique are investigated. The volume fractions of mechanically different phases obtained from statistical analysis are shown to be different from those obtained by back-scattered electron image analysis and X-ray diffraction method on the same paste. Judging from transmission electron microscope images, the representative volume element of low-density calcium-silicate hydrates can be considered to be around 500 nm, whereas for high-density C-S-H it is about 100 nm. This raises the question how the appropriate penetration depth for NI experiments should be selected. Changing the maximum load from 1 mN to 5 mN, the effect of penetration depth on the experimental results is studied. As an alternative, a %22manual%22 indentation method is proposed. (en)
Title
  • Critical Aspects of Nano-Indentation Technique in Application to Hardened Cement Paste
  • Critical Aspects of Nano-Indentation Technique in Application to Hardened Cement Paste (en)
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  • Critical Aspects of Nano-Indentation Technique in Application to Hardened Cement Paste
  • Critical Aspects of Nano-Indentation Technique in Application to Hardened Cement Paste (en)
skos:notation
  • RIV/68407700:21110/11:00171624!RIV12-MSM-21110___
http://linked.open...avai/predkladatel
http://linked.open...avai/riv/aktivita
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  • Z(MSM6840770003)
http://linked.open...iv/cisloPeriodika
  • 1
http://linked.open...vai/riv/dodaniDat
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  • 192263
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  • RIV/68407700:21110/11:00171624
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • calcium-silicate hydrate; elastic modulus; micromechanics; mechanical properties; statistical nanoindentation (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • US - Spojené státy americké
http://linked.open...ontrolniKodProRIV
  • [811E1CFDF2E6]
http://linked.open...i/riv/nazevZdroje
  • Cement and Concrete Research
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
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http://linked.open...UplatneniVysledku
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  • 41
http://linked.open...iv/tvurceVysledku
  • Davydov, Denis
  • Jirásek, Milan
  • Kopecký, Lubomír
http://linked.open...ain/vavai/riv/wos
  • 000285900500003
http://linked.open...n/vavai/riv/zamer
issn
  • 0008-8846
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.cemconres.2010.09.001
http://localhost/t...ganizacniJednotka
  • 21110
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