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  • A new oxidovanadium(IV) Schiff base complex, VOL2 (1), containing furfuryl pendant group was synthesized by the reaction of the related bidentate O,N-type Schiff base ligand and VO(acac)2. The Schiff base ligand and its vanadyl complex were characterized by 1H-NMR and FT-IR spectra and elemental analysis. The crystal structure of 1 was also determined the single-crystal X-ray analysis. The catalytic activity of the vanadyl Schiff base complex was elucidated in the epoxidation of cyclooctene as a model substrate. In addition, the vanadyl Schiff base complex (1) was thermally decomposed in air at 6 60 deg C and the XRD pattern of the obtained solid showed the formation of the V2O5 nanoparticles with the average size of 52 nm.
  • A new oxidovanadium(IV) Schiff base complex, VOL2 (1), containing furfuryl pendant group was synthesized by the reaction of the related bidentate O,N-type Schiff base ligand and VO(acac)2. The Schiff base ligand and its vanadyl complex were characterized by 1H-NMR and FT-IR spectra and elemental analysis. The crystal structure of 1 was also determined the single-crystal X-ray analysis. The catalytic activity of the vanadyl Schiff base complex was elucidated in the epoxidation of cyclooctene as a model substrate. In addition, the vanadyl Schiff base complex (1) was thermally decomposed in air at 6 60 deg C and the XRD pattern of the obtained solid showed the formation of the V2O5 nanoparticles with the average size of 52 nm. (en)
Title
  • Synthesis, characterization, crystal structure determination, catalytic activity and thermal study of a new oxidovanadium(IV) Schiff base complex: production of V2O5 nano-particles
  • Synthesis, characterization, crystal structure determination, catalytic activity and thermal study of a new oxidovanadium(IV) Schiff base complex: production of V2O5 nano-particles (en)
skos:prefLabel
  • Synthesis, characterization, crystal structure determination, catalytic activity and thermal study of a new oxidovanadium(IV) Schiff base complex: production of V2O5 nano-particles
  • Synthesis, characterization, crystal structure determination, catalytic activity and thermal study of a new oxidovanadium(IV) Schiff base complex: production of V2O5 nano-particles (en)
skos:notation
  • RIV/68378271:_____/14:00434839!RIV15-AV0-68378271
http://linked.open...avai/riv/aktivita
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  • I
http://linked.open...iv/cisloPeriodika
  • 4
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http://linked.open...aciTvurceVysledku
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  • 49008
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  • RIV/68378271:_____/14:00434839
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  • uranium complex; isothiosemicarbazone; crystallography; spectra; thermal stability (en)
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  • IR - Íránská islámská republika
http://linked.open...ontrolniKodProRIV
  • [BCB00D80747A]
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  • Journal of the Iranian Chemical Society
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  • 11
http://linked.open...iv/tvurceVysledku
  • Dušek, Michal
  • Fejfarová, Karla
  • Khalaji, A. D.
  • Grivani, G.
  • Delkosh, S.
  • Tahmasebi, V.
http://linked.open...ain/vavai/riv/wos
  • 000337597000002
issn
  • 1735-207X
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http://bibframe.org/vocab/doi
  • 10.1007/s13738-013-0361-y
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