About: A new copper(I) coordination polymer with N2-donor schiff base and Its use as precursor for CuO nanoparticle: Spectroscopic, thermal and structural studies     Goto   Sponge   NotDistinct   Permalink

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  • A new copper(I) coordination polymer, [Cu((3,4-MeO-ba)2bn)I]n (1), using a bridging Schiff base ligand, N,N0-bis(3,4-dimethoxybenzylidene)butane-1,4-diamine, (3,4-MeO-ba)2bn, containing a flexible spacer (=N–CH2–CH2–CH2–CH2–N=) has been synthesized and characterized by elemental analyses (CHN) and FTIR spectroscopy, thermal analysis and powder X-ray structure analysis. In 1, Cu(I) ions are bridged by Schiff base ligands and iodine atoms forming 1D-chain. The thermal stability of 1 was studied by thermal gravimetric and differential thermal analyses. 1 is used to prepare CuO nanoparticles via solid state thermal decomposition in air and nanoparticles thus formed are characterized by scanning electron microscopy, transmission electron microscopy and powder X-ray diffraction techniques.
  • A new copper(I) coordination polymer, [Cu((3,4-MeO-ba)2bn)I]n (1), using a bridging Schiff base ligand, N,N0-bis(3,4-dimethoxybenzylidene)butane-1,4-diamine, (3,4-MeO-ba)2bn, containing a flexible spacer (=N–CH2–CH2–CH2–CH2–N=) has been synthesized and characterized by elemental analyses (CHN) and FTIR spectroscopy, thermal analysis and powder X-ray structure analysis. In 1, Cu(I) ions are bridged by Schiff base ligands and iodine atoms forming 1D-chain. The thermal stability of 1 was studied by thermal gravimetric and differential thermal analyses. 1 is used to prepare CuO nanoparticles via solid state thermal decomposition in air and nanoparticles thus formed are characterized by scanning electron microscopy, transmission electron microscopy and powder X-ray diffraction techniques. (en)
Title
  • A new copper(I) coordination polymer with N2-donor schiff base and Its use as precursor for CuO nanoparticle: Spectroscopic, thermal and structural studies
  • A new copper(I) coordination polymer with N2-donor schiff base and Its use as precursor for CuO nanoparticle: Spectroscopic, thermal and structural studies (en)
skos:prefLabel
  • A new copper(I) coordination polymer with N2-donor schiff base and Its use as precursor for CuO nanoparticle: Spectroscopic, thermal and structural studies
  • A new copper(I) coordination polymer with N2-donor schiff base and Its use as precursor for CuO nanoparticle: Spectroscopic, thermal and structural studies (en)
skos:notation
  • RIV/68378271:_____/14:00434249!RIV15-AV0-68378271
http://linked.open...avai/riv/aktivita
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  • I
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  • 5
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  • 882
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  • RIV/68378271:_____/14:00434249
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  • copper(I) complex; schiff base; spectroscopy; thermal study; nanoparticle; SEM; XRD (en)
http://linked.open.../riv/klicoveSlovo
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  • US - Spojené státy americké
http://linked.open...ontrolniKodProRIV
  • [6B25F44B645B]
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  • Journal of Cluster Science
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  • 25
http://linked.open...iv/tvurceVysledku
  • Das, D.
  • Khalaji, A. D.
  • Rohlíček, Jan
  • Machek, Pavel
http://linked.open...ain/vavai/riv/wos
  • 000342115700020
issn
  • 1040-7278
number of pages
http://bibframe.org/vocab/doi
  • 10.1007/s10876-014-0719-z
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