About: Synthesis, crystal structure, antimicrobial activity and electrochemistry study of chromium(III) and copper(II) complexes based on semicarbazone Schiff base and azide ligands     Goto   Sponge   NotDistinct   Permalink

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  • A tridentate NNO donor Schiff base ligand HL=C5H4NCH=NNHCONH2 was obtained by condensation of pyridine 2-carbaldehyde with semicarbazide. The HL and azide ligands with Cr(III) and Cu(II) ions have been used to synthesize a dinuclear complex [Cr(L)(N3)(OCH3)]2 (1) and a coordination polymer complex [Cu(L)(N3)]n (2). The ligand, 1 and 2 were clearly characterised by elemental analysis, FT-IR, UV–Vis spectral studies and the structures of the 1 and 2, have been studied by single crystal X-ray diffraction analysis.
  • A tridentate NNO donor Schiff base ligand HL=C5H4NCH=NNHCONH2 was obtained by condensation of pyridine 2-carbaldehyde with semicarbazide. The HL and azide ligands with Cr(III) and Cu(II) ions have been used to synthesize a dinuclear complex [Cr(L)(N3)(OCH3)]2 (1) and a coordination polymer complex [Cu(L)(N3)]n (2). The ligand, 1 and 2 were clearly characterised by elemental analysis, FT-IR, UV–Vis spectral studies and the structures of the 1 and 2, have been studied by single crystal X-ray diffraction analysis. (en)
Title
  • Synthesis, crystal structure, antimicrobial activity and electrochemistry study of chromium(III) and copper(II) complexes based on semicarbazone Schiff base and azide ligands
  • Synthesis, crystal structure, antimicrobial activity and electrochemistry study of chromium(III) and copper(II) complexes based on semicarbazone Schiff base and azide ligands (en)
skos:prefLabel
  • Synthesis, crystal structure, antimicrobial activity and electrochemistry study of chromium(III) and copper(II) complexes based on semicarbazone Schiff base and azide ligands
  • Synthesis, crystal structure, antimicrobial activity and electrochemistry study of chromium(III) and copper(II) complexes based on semicarbazone Schiff base and azide ligands (en)
skos:notation
  • RIV/68378271:_____/13:00391607!RIV14-AV0-68378271
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  • 109508
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  • RIV/68378271:_____/13:00391607
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  • antimicrobial activity; azide ligand; metal complex; Schiff base ligand; X-ray structure (en)
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  • NL - Nizozemsko
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  • Inorganica chimica acta
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  • 394
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  • Dušek, Michal
  • Pojarová, Michaela
  • Khandar, A. A.
  • Mahmoudi, F.
  • Shaabani, B.
http://linked.open...ain/vavai/riv/wos
  • 000311492900075
issn
  • 0020-1693
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.ica.2012.08.027
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