About: Minimization of absorption contrast for accurate amorphous phase quantification: application to ZrO2 nanoparticles

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Monoclinic and tetragonal zirconia samples were characterized by X-ray diffraction, pycnometry, thermogravimetric analysis (TGA), Fourier transform (FT) IR and mass (MS) spectroscopies, and scanning and transmission electron (TEM) microscopies. The results show, for the particular case of a tetragonal zirconia sample, an X-ray-undetected subproduct identified as an amorphous organic phase by FTIR–ATR (attenuated total reflection) and TGA–MS. The observations by TEM allowed this amorphous phase to be localized on the surface as a shell coating the nanoparticles. Moreover, this amorphous phase was quantified by Rietveld refinement via the addition of an internal silicon standard. Monoclinic and tetragonal zirconia samples were characterized by X-ray diffraction, pycnometry, thermogravimetric analysis (TGA), Fourier transform (FT) IR and mass (MS) spectroscopies, and scanning and transmission electron (TEM) microscopies. The results show, for the particular case of a tetragonal zirconia sample, an X-ray-undetected subproduct identified as an amorphous organic phase by FTIR–ATR (attenuated total reflection) and TGA–MS. The observations by TEM allowed this amorphous phase to be localized on the surface as a shell coating the nanoparticles. Moreover, this amorphous phase was quantified by Rietveld refinement via the addition of an internal silicon standard. (en)
Title	Minimization of absorption contrast for accurate amorphous phase quantification: application to ZrO2 nanoparticles Minimization of absorption contrast for accurate amorphous phase quantification: application to ZrO2 nanoparticles (en)
skos:prefLabel	Minimization of absorption contrast for accurate amorphous phase quantification: application to ZrO2 nanoparticles Minimization of absorption contrast for accurate amorphous phase quantification: application to ZrO2 nanoparticles (en)
skos:notation	RIV/68378271:_____/10:00349618!RIV11-AV0-68378271
http://linked.open...avai/riv/aktivita	Z
http://linked.open...avai/riv/aktivity	Z(AV0Z10100521)
http://linked.open...iv/cisloPeriodika	Part 5
http://linked.open...vai/riv/dodaniDat	2011
http://linked.open...aciTvurceVysledku	Petříček, Václav
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Fyzikální ústav AV ČR, v. v. i.
http://linked.open...dnocenehoVysledku	271517
http://linked.open...ai/riv/idVysledku	RIV/68378271:_____/10:00349618
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	x-ray diffraction; Rietveld refinement; nanoparticles (en)
http://linked.open.../riv/klicoveSlovo	nanoparticles x-ray diffraction Rietveld refinement
http://linked.open...odStatuVydavatele	GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV	[067A135DD81F]
http://linked.open...i/riv/nazevZdroje	Journal of Applied Crystallography
http://linked.open...in/vavai/riv/obor	BM
http://linked.open...ichTvurcuVysledku	1 (xsd:int)
http://linked.open...cetTvurcuVysledku	6 (xsd:int)
http://linked.open...UplatneniVysledku	2010
http://linked.open...v/svazekPeriodika	43
http://linked.open...iv/tvurceVysledku	Petříček, Václav Gautron, E. Deniard, P. Grambow, B. Jobic, S. Suzuki-Muresan, T.
http://linked.open...ain/vavai/riv/wos	000281996600021
http://linked.open...n/vavai/riv/zamer	Physics and technology of nanostructures, surfaces and thin films
issn	0021-8898
number of pages	8 (xsd:int)
is http://linked.open...avai/riv/vysledek of	Minimization of absorption contrast for accurate amorphous phase quantification: application to ZrO2 nanoparticles Minimization of absorption contrast for accurate amorphous phase quantification: application to ZrO2 nanoparticles Minimization of absorption contrast for accurate amorphous phase quantification: application to ZrO2 nanoparticles

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