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  • Stable Pd nanoparticles (PdNP) with a tunable size (3-15 nm) were synthesized by controlled chemical reduction of PdCl2 with sodium citrate in water. The morphology of PdNP was characterized by transmission electron microscopy, while their stability in solution was verified by quasi-elastic light scattering and small-angle X-ray scattering. Intensive stirring of reacting mixture played a vital role in achieving reproducible particle sizes. Controlled changes of pH and initial concentrations were employed in fine-tuning particle size distributions. Finally, 10 nm PdNP were conjugated with goat anti-mouse IgG antibody as proved by electrophoresis (SOS-PAGE) and used for ultrastructural immunolabeling, which confirmed suitability of PdNP for multiple immunolabeling in biomedicine.
  • Stable Pd nanoparticles (PdNP) with a tunable size (3-15 nm) were synthesized by controlled chemical reduction of PdCl2 with sodium citrate in water. The morphology of PdNP was characterized by transmission electron microscopy, while their stability in solution was verified by quasi-elastic light scattering and small-angle X-ray scattering. Intensive stirring of reacting mixture played a vital role in achieving reproducible particle sizes. Controlled changes of pH and initial concentrations were employed in fine-tuning particle size distributions. Finally, 10 nm PdNP were conjugated with goat anti-mouse IgG antibody as proved by electrophoresis (SOS-PAGE) and used for ultrastructural immunolabeling, which confirmed suitability of PdNP for multiple immunolabeling in biomedicine. (en)
Title
  • Preparation of stable Pd nanoparticles with tunable size for multiple immunolabeling in biomedicine
  • Preparation of stable Pd nanoparticles with tunable size for multiple immunolabeling in biomedicine (en)
skos:prefLabel
  • Preparation of stable Pd nanoparticles with tunable size for multiple immunolabeling in biomedicine
  • Preparation of stable Pd nanoparticles with tunable size for multiple immunolabeling in biomedicine (en)
skos:notation
  • RIV/68378050:_____/11:00359122!RIV12-AV0-68378050
http://linked.open...avai/predkladatel
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GAP205/10/0348), P(KAN200520704), Z(AV0Z40500505), Z(AV0Z50520514)
http://linked.open...iv/cisloPeriodika
  • 8
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 223103
http://linked.open...ai/riv/idVysledku
  • RIV/68378050:_____/11:00359122
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • palladium nanoparticles; nanocrystalline materials; immunolabeling (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [69B9B1694756]
http://linked.open...i/riv/nazevZdroje
  • Materials Letters
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 65
http://linked.open...iv/tvurceVysledku
  • Hozák, Pavel
  • Šlouf, Miroslav
  • Pleštil, Josef
  • Pavlova, Ewa
  • Philimonenko, Anatoly
  • Bhardwaj, Monika
  • Onderková, H.
http://linked.open...ain/vavai/riv/wos
  • 000288928500017
http://linked.open...n/vavai/riv/zamer
issn
  • 0167-577X
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.matlet.2011.01.046
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