About: HCSE Method for Detection of Small Carbo-Carbon Couplings and Their Signs, Comparison with SLAP Pulse Sequence

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Description	Performance of HCSE experiment applied to detection of signed carbon-carbon couplings is discussed using a set of already measured samples of 9 monosubstituted benzenes. It is shown that coupling sign detection is insensitive to the settings of carbon-carbon polarization transfer delays. The HCSE spectra of 10 from the total of 43 measured carbon-carbon couplings were considerably influenced by relaxations and proton-proton strong couplings. These effects are quantitatively discussed. The results of HCSE and SLAP experiments are compared. It is shown that the two methods may complement each other in detection of signed carbon-carbon couplings. Performance of HCSE experiment applied to detection of signed carbon-carbon couplings is discussed using a set of already measured samples of 9 monosubstituted benzenes. It is shown that coupling sign detection is insensitive to the settings of carbon-carbon polarization transfer delays. The HCSE spectra of 10 from the total of 43 measured carbon-carbon couplings were considerably influenced by relaxations and proton-proton strong couplings. These effects are quantitatively discussed. The results of HCSE and SLAP experiments are compared. It is shown that the two methods may complement each other in detection of signed carbon-carbon couplings. (en)
Title	HCSE Method for Detection of Small Carbo-Carbon Couplings and Their Signs, Comparison with SLAP Pulse Sequence HCSE Method for Detection of Small Carbo-Carbon Couplings and Their Signs, Comparison with SLAP Pulse Sequence (en)
skos:prefLabel	HCSE Method for Detection of Small Carbo-Carbon Couplings and Their Signs, Comparison with SLAP Pulse Sequence HCSE Method for Detection of Small Carbo-Carbon Couplings and Their Signs, Comparison with SLAP Pulse Sequence (en)
skos:notation	RIV/67985858:_____/13:00424661!RIV14-TA0-67985858
http://linked.open...avai/predkladatel	Ústav chemických procesů Akademie Věd ČR, v.v.i.
http://linked.open...avai/riv/aktivita	I P
http://linked.open...avai/riv/aktivity	I, P(TA01010646)
http://linked.open...iv/cisloPeriodika	11
http://linked.open...vai/riv/dodaniDat	2014
http://linked.open...aciTvurceVysledku	Schraml, Jan Blechta, Vratislav
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Ústav chemických procesů AV ČR, v. v. i.
http://linked.open...dnocenehoVysledku	77103
http://linked.open...ai/riv/idVysledku	RIV/67985858:_____/13:00424661
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	coupling sign; HCSE; SLAP (en)
http://linked.open.../riv/klicoveSlovo	HCSE SLAP coupling sign
http://linked.open...odStatuVydavatele	GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV	[5F508C3180A9]
http://linked.open...i/riv/nazevZdroje	Magnetic Resonance in Chemistry
http://linked.open...in/vavai/riv/obor	CC
http://linked.open...ichTvurcuVysledku	2 (xsd:int)
http://linked.open...cetTvurcuVysledku	2 (xsd:int)
http://linked.open...vavai/riv/projekt	Preparation of helicene based chiral stationary phase for HPLC
http://linked.open...UplatneniVysledku	2013
http://linked.open...v/svazekPeriodika	51
http://linked.open...iv/tvurceVysledku	Schraml, Jan Blechta, Vratislav
http://linked.open...ain/vavai/riv/wos	000325262200010
issn	0749-1581
number of pages	7 (xsd:int)
http://bibframe.org/vocab/doi	10.1002/mrc.4011

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