About: Supercritical Fluid Extraction of Lignans and Cinnamic Acid from Schizandra chinensis.     Goto   Sponge   NotDistinct   Permalink

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  • Biologically active lignans from caulomas (stems) and leaves of Schisandra chinensis were extracted with supercritical carbon dioxide at the pressures 20–27 MPa, temperatures 40, 50 and 60 C, and solvent-to-feed ratio 36–43. Six major lignans were determined by means of HPLC: schizandrin, gomisin A, deoxyschizandrin, g-schizandrin, gomisin N and wuweizisu C. At the optimum conditions 27 MPa and 50 C, the extraction yield of lignans from caulomas was 1.3% dry weight and their content in the extract was higher than 32 wt.%. At the optimum conditions for CO2 extraction from S. chinensis leaves, 27MPa and 60 C, the yield of lignans was 0.22% d.w. and the yield of (E)-cinnamic acid was 0.18% d.w. Addition of 2–4% ethanol to CO2 increased the extraction rate but not the final yield of lignans. The solubility of extracted substances in supercritical CO2 was estimated from their extraction rates.
  • Biologically active lignans from caulomas (stems) and leaves of Schisandra chinensis were extracted with supercritical carbon dioxide at the pressures 20–27 MPa, temperatures 40, 50 and 60 C, and solvent-to-feed ratio 36–43. Six major lignans were determined by means of HPLC: schizandrin, gomisin A, deoxyschizandrin, g-schizandrin, gomisin N and wuweizisu C. At the optimum conditions 27 MPa and 50 C, the extraction yield of lignans from caulomas was 1.3% dry weight and their content in the extract was higher than 32 wt.%. At the optimum conditions for CO2 extraction from S. chinensis leaves, 27MPa and 60 C, the yield of lignans was 0.22% d.w. and the yield of (E)-cinnamic acid was 0.18% d.w. Addition of 2–4% ethanol to CO2 increased the extraction rate but not the final yield of lignans. The solubility of extracted substances in supercritical CO2 was estimated from their extraction rates. (en)
  • Biologicky aktivní lignany byly extrahovány z kaulomů (stonků) a listů Schisandry chinensis superkritickým oxidem uhličitým při tlaku 20-27 MPa, teplotě 40, 50 a 60 C, a poměru rozpouštědla k navážce 36-43 g/g. Kapalinovou chromatografií bylo stanoveno 6 hlavních lignanů: schizandrin, gomisin A, deoxyschizandrin, g-schizandrin, gomisin N a wuweizisu C. Při extrakci z kaulomů byly optimální podmínky 27 MPa a 50 C, výtěžek lignanů byl 1,3 % sušiny a jejich obsah v extraktu byl větší než 32 %. Při extrakci z listů byly optimální podmínky 27 MPa a 60 C, výtěžek lignanů byl 0,22 % sušiny a výtěžek kyseliny skořicové byl 0,18 % sušiny. Přídavkem 2-4 % etanolu k CO2 vzrostla rychlost extrakce, ale nezvýšil se konečný výtěžek lignanů. Z extrakční rychlosti byla vyhodnocena rozpustnost jednotlivých složek v superkritickém CO2. (cs)
Title
  • Supercritical Fluid Extraction of Lignans and Cinnamic Acid from Schizandra chinensis.
  • Supercritical Fluid Extraction of Lignans and Cinnamic Acid from Schizandra chinensis. (en)
  • Superkritická extrakce lignanů a kyseliny skořicové ze Schisandry chinensis. (cs)
skos:prefLabel
  • Supercritical Fluid Extraction of Lignans and Cinnamic Acid from Schizandra chinensis.
  • Supercritical Fluid Extraction of Lignans and Cinnamic Acid from Schizandra chinensis. (en)
  • Superkritická extrakce lignanů a kyseliny skořicové ze Schisandry chinensis. (cs)
skos:notation
  • RIV/67985858:_____/07:00091190!RIV08-AV0-67985858
http://linked.open.../vavai/riv/strany
  • 88;95
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA203/01/0550), P(IAA4072102), P(KSK4040110), V, Z(AV0Z40720504)
http://linked.open...iv/cisloPeriodika
  • 1
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 453520
http://linked.open...ai/riv/idVysledku
  • RIV/67985858:_____/07:00091190
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • supercritical extraction; solubility; lignans (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [A81D0DD3E7D2]
http://linked.open...i/riv/nazevZdroje
  • Journal of Supercritical Fluids
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 42
http://linked.open...iv/tvurceVysledku
  • Opletal, L.
  • Sovová, Helena
  • Sajfrtová, Marie
  • Bártlová, Milena
  • Křenková, M.
http://linked.open...n/vavai/riv/zamer
issn
  • 0896-8446
number of pages
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