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Description
  • A new procedure for the preparation of macrocycles containing 1,2,3-triazole motifs is developed. The macrocyclic precursor is constructed by repetition of a series of steps which include cycloaddition of an azide with an alkyne, alkylation of a carboxylic acid with propargyl bromide and formation of an azide from an amino group. The order of the steps and the size of the connected fragments are determined by the desired ring size. Chromatographic purification techniques for the poorly soluble final products are also described.
  • A new procedure for the preparation of macrocycles containing 1,2,3-triazole motifs is developed. The macrocyclic precursor is constructed by repetition of a series of steps which include cycloaddition of an azide with an alkyne, alkylation of a carboxylic acid with propargyl bromide and formation of an azide from an amino group. The order of the steps and the size of the connected fragments are determined by the desired ring size. Chromatographic purification techniques for the poorly soluble final products are also described. (en)
Title
  • Synthesis of macrocycles containing 1,2,3-triazole motifs
  • Synthesis of macrocycles containing 1,2,3-triazole motifs (en)
skos:prefLabel
  • Synthesis of macrocycles containing 1,2,3-triazole motifs
  • Synthesis of macrocycles containing 1,2,3-triazole motifs (en)
skos:notation
  • RIV/62690094:18470/12:50000941!RIV13-MSM-18470___
http://linked.open...avai/predkladatel
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • N, P(ME09057)
http://linked.open...iv/cisloPeriodika
  • 9
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
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  • 172968
http://linked.open...ai/riv/idVysledku
  • RIV/62690094:18470/12:50000941
http://linked.open...riv/jazykVysledku
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  • propargyl ester; azidobenzoate; cycloaddition; 1,2,3-triazole; Macrocycles (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [CD0818AACFDC]
http://linked.open...i/riv/nazevZdroje
  • Synthesis
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
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http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 44
http://linked.open...iv/tvurceVysledku
  • Hlaváč, Jan
  • Grepl, Martin
  • Hradil, Pavel
  • Lyčka, Antonín
  • Hradilová, Ludmila
http://linked.open...ain/vavai/riv/wos
  • 000303104500017
issn
  • 0039-7881
number of pages
http://bibframe.org/vocab/doi
  • 10.1055/s-0031-1290760
http://localhost/t...ganizacniJednotka
  • 18470
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