About: Study of direct macrocycle formation via the cyclisation of propargyl 2-azidobenzoate

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Macrocycles were synthesised via the cyclisation of propargyl 2-azidobenzoate using 'click' chemistry. An LC/MS-based method for the separation of macrocycles is described. In the present work, the influence of various catalysts and reaction conditions on the course of the reaction is evaluated. The reaction is very sensitive to the conditions, and it is demonstrated that it is possible to modify the ratio of macrocycles by varying the reaction conditions. The cyclisation of propargyl 2-azidobenzoate represents an economical method for the preparation of the studied macrocycles Macrocycles were synthesised via the cyclisation of propargyl 2-azidobenzoate using 'click' chemistry. An LC/MS-based method for the separation of macrocycles is described. In the present work, the influence of various catalysts and reaction conditions on the course of the reaction is evaluated. The reaction is very sensitive to the conditions, and it is demonstrated that it is possible to modify the ratio of macrocycles by varying the reaction conditions. The cyclisation of propargyl 2-azidobenzoate represents an economical method for the preparation of the studied macrocycles (en)
Title	Study of direct macrocycle formation via the cyclisation of propargyl 2-azidobenzoate Study of direct macrocycle formation via the cyclisation of propargyl 2-azidobenzoate (en)
skos:prefLabel	Study of direct macrocycle formation via the cyclisation of propargyl 2-azidobenzoate Study of direct macrocycle formation via the cyclisation of propargyl 2-azidobenzoate (en)
skos:notation	RIV/61989592:15310/13:33147718!RIV15-MSM-15310___
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(ME09057), Z(MSM6198959216)
http://linked.open...iv/cisloPeriodika	10
http://linked.open...vai/riv/dodaniDat	2015
http://linked.open...aciTvurceVysledku	Hradil, Pavel
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Univerzita Palackého v Olomouci / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	108674
http://linked.open...ai/riv/idVysledku	RIV/61989592:15310/13:33147718
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	Macrocycles; LC/MS; Cyclisation; Click reaction; 2-Azidobenzoate (en)
http://linked.open.../riv/klicoveSlovo	LC/MS 2-Azidobenzoate Cyclisation Click reaction Macrocycles
http://linked.open...odStatuVydavatele	GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV	[B0297722B82E]
http://linked.open...i/riv/nazevZdroje	Tetrahedron Letters
http://linked.open...in/vavai/riv/obor	CC
http://linked.open...ichTvurcuVysledku	1 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...vavai/riv/projekt	Research of new organic compounds with anticancer activity with use of combinatorial chemistry
http://linked.open...UplatneniVysledku	2013
http://linked.open...v/svazekPeriodika	54
http://linked.open...iv/tvurceVysledku	Grepl, Martin Hradil, Pavel Dvořáková, Barbora Hradilová, Ludmila
http://linked.open...ain/vavai/riv/wos	000315321600010
http://linked.open...n/vavai/riv/zamer	Modulation of signalling and regulatory pathways in normal and cancer cells
issn	0040-4039
number of pages	4 (xsd:int)
http://bibframe.org/vocab/doi	10.1016/j.tetlet.2012.12.076
http://localhost/t...ganizacniJednotka	15310

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