About: Synthesis of 1-Aminocodeine as a Synthon for Other Codeine Derivatives     Goto   Sponge   NotDistinct   Permalink

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Description
  • The first nitration of codeine by using bismuth nitrate pentahydrate under mild reaction conditions is described. The resulting 1-nitrocodeine was reduced to 1-aminocodeine, a key precursor for the synthesis of the azo derivative and several hydrazones. Structures of both 1-nitrocodeine and 1-amino-codeine were unequivocally determined by single-crystal Xray analysis. The reported preliminary synthetic study lays the groundwork for the synthesis of modified codeine derivatives with potential biological activity.
  • The first nitration of codeine by using bismuth nitrate pentahydrate under mild reaction conditions is described. The resulting 1-nitrocodeine was reduced to 1-aminocodeine, a key precursor for the synthesis of the azo derivative and several hydrazones. Structures of both 1-nitrocodeine and 1-amino-codeine were unequivocally determined by single-crystal Xray analysis. The reported preliminary synthetic study lays the groundwork for the synthesis of modified codeine derivatives with potential biological activity. (en)
Title
  • Synthesis of 1-Aminocodeine as a Synthon for Other Codeine Derivatives
  • Synthesis of 1-Aminocodeine as a Synthon for Other Codeine Derivatives (en)
skos:prefLabel
  • Synthesis of 1-Aminocodeine as a Synthon for Other Codeine Derivatives
  • Synthesis of 1-Aminocodeine as a Synthon for Other Codeine Derivatives (en)
skos:notation
  • RIV/61989592:15310/13:33147715!RIV15-MSM-15310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(ED2.1.00/03.0058), P(EE2.3.20.0017), P(EE2.4.31.0130)
http://linked.open...iv/cisloPeriodika
  • 17
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 109560
http://linked.open...ai/riv/idVysledku
  • RIV/61989592:15310/13:33147715
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Synthetic methods / Drug design / Fused-ring systems / Diazo compounds / Isotopic labelling / Reduction (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [08AFB91D0A79]
http://linked.open...i/riv/nazevZdroje
  • European Journal of Organic Chemistry
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 2013
http://linked.open...iv/tvurceVysledku
  • Trávníček, Zdeněk
  • Hradil, Pavel
  • Popa, Igor
  • Cankař, Petr
  • Stýskala, Jakub
  • Slouka, Jan
http://linked.open...ain/vavai/riv/wos
  • 000324302600011
issn
  • 1434-193X
number of pages
http://bibframe.org/vocab/doi
  • 10.1002/ejoc.201300701
http://localhost/t...ganizacniJednotka
  • 15310
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