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  • Methods of determination of selenium in samples of dilute and mineralized blood serum by AAS with electrothermal atomization and hydride generation are described. Use of various matrix modifiers (Pd(NO3)(2) + Mg(NO3)(2), Ni(NO3)(2) + Mg(NO3)(2) and Pd + ascorbic acid) and introduction of air into a furnace during pyrolysis are discussed. With hydride generation, the influence of interfering substances (sodium and HNO3 residues after mineralizations) and optimization of the quartz atomization tube temperature are described. For all procedures, the limits of detection, determination and repeatability as well as the results of analysis of a reference material (Seronorm(TM) Trace Element Serum) and of reversibility testing are given.
  • Methods of determination of selenium in samples of dilute and mineralized blood serum by AAS with electrothermal atomization and hydride generation are described. Use of various matrix modifiers (Pd(NO3)(2) + Mg(NO3)(2), Ni(NO3)(2) + Mg(NO3)(2) and Pd + ascorbic acid) and introduction of air into a furnace during pyrolysis are discussed. With hydride generation, the influence of interfering substances (sodium and HNO3 residues after mineralizations) and optimization of the quartz atomization tube temperature are described. For all procedures, the limits of detection, determination and repeatability as well as the results of analysis of a reference material (Seronorm(TM) Trace Element Serum) and of reversibility testing are given. (en)
Title
  • Optimization of conditions of selenium determination in blood serum by atomic absorption spectrometry
  • Optimization of conditions of selenium determination in blood serum by atomic absorption spectrometry (en)
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  • Optimization of conditions of selenium determination in blood serum by atomic absorption spectrometry
  • Optimization of conditions of selenium determination in blood serum by atomic absorption spectrometry (en)
skos:notation
  • RIV/61989592:15310/02:00001587!RIV/2003/MSM/153103/N
http://linked.open.../vavai/riv/strany
  • 708-712
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM 153100013)
http://linked.open...iv/cisloPeriodika
  • 8
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
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  • 657325
http://linked.open...ai/riv/idVysledku
  • RIV/61989592:15310/02:00001587
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  • blood serum; atomic absorption spectrometry (en)
http://linked.open.../riv/klicoveSlovo
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  • CZ - Česká republika
http://linked.open...ontrolniKodProRIV
  • [4820AE15D38F]
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  • Chemické listy
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http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 96
http://linked.open...iv/tvurceVysledku
  • Milde, David
  • Macháček, Jindřich
  • Stužka, Václav
  • Šobrová, Markéta
http://linked.open...n/vavai/riv/zamer
issn
  • 0009-2770
number of pages
http://localhost/t...ganizacniJednotka
  • 15310
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