About: Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In situ characterisation of Renaissance plates by portable micro-Raman and XRF studies     Goto   Sponge   NotDistinct   Permalink

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  • The effectiveness of Raman spectroscopy (using a bench-top system on standard pigments) for the characterisation of modified lead antimonate yellows was demonstrated in the already published Part I. The knowledge gained is employed here for the study of yellow glazes on genuine Renaissance plates with the aim of identifying non-invasively lead pyroantimonate compounds by portable micro-Raman equipment. The investigation was carried out directly on site, at the Victoria and Albert Museum (London, UK) and at the Museo Statale d'Arte Medievale di Arezzo (Arezzo, Italy), combining Raman and X-ray fluorescence analyses. In addition to the spectral features of both unmodified Naples yellow and Sn- and Zn-modified lead antimonate compounds, the Raman patterns related to partially modified pyrochlore structures were observed. For this reason, the possible Sn-induced modification of Naples yellow by cassiterite (SnO(2)), present within the glaze as opacifier was explored on lead antimonate yellow glaze mock-ups fired at different temperatures.
  • The effectiveness of Raman spectroscopy (using a bench-top system on standard pigments) for the characterisation of modified lead antimonate yellows was demonstrated in the already published Part I. The knowledge gained is employed here for the study of yellow glazes on genuine Renaissance plates with the aim of identifying non-invasively lead pyroantimonate compounds by portable micro-Raman equipment. The investigation was carried out directly on site, at the Victoria and Albert Museum (London, UK) and at the Museo Statale d'Arte Medievale di Arezzo (Arezzo, Italy), combining Raman and X-ray fluorescence analyses. In addition to the spectral features of both unmodified Naples yellow and Sn- and Zn-modified lead antimonate compounds, the Raman patterns related to partially modified pyrochlore structures were observed. For this reason, the possible Sn-induced modification of Naples yellow by cassiterite (SnO(2)), present within the glaze as opacifier was explored on lead antimonate yellow glaze mock-ups fired at different temperatures. (en)
Title
  • Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In situ characterisation of Renaissance plates by portable micro-Raman and XRF studies
  • Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In situ characterisation of Renaissance plates by portable micro-Raman and XRF studies (en)
skos:prefLabel
  • Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In situ characterisation of Renaissance plates by portable micro-Raman and XRF studies
  • Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In situ characterisation of Renaissance plates by portable micro-Raman and XRF studies (en)
skos:notation
  • RIV/61388980:_____/11:00370205!RIV12-AV0-61388980
http://linked.open...avai/predkladatel
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(AV0Z40320502)
http://linked.open...iv/cisloPeriodika
  • 3
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 225648
http://linked.open...ai/riv/idVysledku
  • RIV/61388980:_____/11:00370205
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Naples yellow; lead antimonate; cubic pyrochlore; non-invasive; in situ (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV
  • [025289652544]
http://linked.open...i/riv/nazevZdroje
  • Journal of Raman Spectroscopy
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 42
http://linked.open...iv/tvurceVysledku
  • Bezdička, Petr
  • Grygar, Tomáš
  • Brunetti, B. G.
  • Burgio, L.
  • Manuali, V.
  • Miliani, C.
  • Rosi, F.
  • Seccaroni, C.
  • Sgamellotti, A.
http://linked.open...ain/vavai/riv/wos
  • 000288544000023
http://linked.open...n/vavai/riv/zamer
issn
  • 0377-0486
number of pages
http://bibframe.org/vocab/doi
  • 10.1002/jrs.2699
is http://linked.open...avai/riv/vysledek of
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