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  • Mesoporous titania aerogel with high surfaces area (1086 m(2) g(-1)) were prepared by two steps: heterogeneous precipitation of aqueous solution containing TiOSO4 and ammonia, followed by continuous supercritical extraction with CO2 after replacement of the water with n-propanol/benzene mixture. The total pore volume of as obtained aerogel is 3.44 cm(-3) g(-1) and the main pore diameter is 20-80 nm. The structure evolution of titania aerogel during heating was studied by DTA and high temperature XRD analyses. At 450 degrees C titania aerogel transforms to polycrystalline anatase. The morphology and microstructure characteristics of both titania aerogel and anatase samples were obtained by SEM, HRTEM, BET and BJH methods. Anatase reveals high photocatalytic activity during the degradation of 4-chlorophenol in aqueous suspension.
  • Mesoporous titania aerogel with high surfaces area (1086 m(2) g(-1)) were prepared by two steps: heterogeneous precipitation of aqueous solution containing TiOSO4 and ammonia, followed by continuous supercritical extraction with CO2 after replacement of the water with n-propanol/benzene mixture. The total pore volume of as obtained aerogel is 3.44 cm(-3) g(-1) and the main pore diameter is 20-80 nm. The structure evolution of titania aerogel during heating was studied by DTA and high temperature XRD analyses. At 450 degrees C titania aerogel transforms to polycrystalline anatase. The morphology and microstructure characteristics of both titania aerogel and anatase samples were obtained by SEM, HRTEM, BET and BJH methods. Anatase reveals high photocatalytic activity during the degradation of 4-chlorophenol in aqueous suspension. (en)
  • TiO2 aerogel připravený nízkou teplotou sušení. (cs)
Title
  • Titania aerogel prepared by low temperature supercritical drying
  • Titania aerogel prepared by low temperature supercritical drying (en)
  • TiO2 aerogel připravený nízkou teplotou sušení (cs)
skos:prefLabel
  • Titania aerogel prepared by low temperature supercritical drying
  • Titania aerogel prepared by low temperature supercritical drying (en)
  • TiO2 aerogel připravený nízkou teplotou sušení (cs)
skos:notation
  • RIV/61388980:_____/06:00040429!RIV07-MSM-61388980
http://linked.open.../vavai/riv/strany
  • 1;6
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(1M0577), Z(AV0Z40320502)
http://linked.open...iv/cisloPeriodika
  • 1-3
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 503929
http://linked.open...ai/riv/idVysledku
  • RIV/61388980:_____/06:00040429
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • aerogels; titanium oxide; supercritical drying (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [7586015B429D]
http://linked.open...i/riv/nazevZdroje
  • Microporous and Mesoporous Materials
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 91
http://linked.open...iv/tvurceVysledku
  • Szatmary, Lorant
  • Šubrt, Jan
  • Bakardjieva, Snejana
  • Štengl, Václav
http://linked.open...n/vavai/riv/zamer
issn
  • 1387-1811
number of pages
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