About: X-ray Tomography Imaging of Porous Polyolefin Particles in an Electron Microscope     Goto   Sponge   NotDistinct   Permalink

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Description
  • Advanced models of penetrant transport and reaction in spatially three-dimensional porous polyolefin particles reconstructed from X-ray micro-tomography (micro CT) images require proper determination of particle morphology otherwise the models cannot be validated by experimental data. Moreover, polyolefins exhibit a relatively low absorptivity for X-rays, therefore their investigation using micro CT can be difficult. In this paper, we utilize a low-resolution micro CT built-in a scanning electron microscope (SEM) and examine how the micro CT resolution and several user-selected parameters associated with the scanning/reconstruction affect the resulting particle morphology. Using samples with known morphology and independent imaging techniques (SEM) we critically assess the performance of the micro CT device. Finally, we propose a methodology suitable for the reliable reconstruction of polyolefin particles using low-resolution micro CT.
  • Advanced models of penetrant transport and reaction in spatially three-dimensional porous polyolefin particles reconstructed from X-ray micro-tomography (micro CT) images require proper determination of particle morphology otherwise the models cannot be validated by experimental data. Moreover, polyolefins exhibit a relatively low absorptivity for X-rays, therefore their investigation using micro CT can be difficult. In this paper, we utilize a low-resolution micro CT built-in a scanning electron microscope (SEM) and examine how the micro CT resolution and several user-selected parameters associated with the scanning/reconstruction affect the resulting particle morphology. Using samples with known morphology and independent imaging techniques (SEM) we critically assess the performance of the micro CT device. Finally, we propose a methodology suitable for the reliable reconstruction of polyolefin particles using low-resolution micro CT. (en)
Title
  • X-ray Tomography Imaging of Porous Polyolefin Particles in an Electron Microscope
  • X-ray Tomography Imaging of Porous Polyolefin Particles in an Electron Microscope (en)
skos:prefLabel
  • X-ray Tomography Imaging of Porous Polyolefin Particles in an Electron Microscope
  • X-ray Tomography Imaging of Porous Polyolefin Particles in an Electron Microscope (en)
skos:notation
  • RIV/60461373:22340/13:43895650!RIV14-GA0-22340___
http://linked.open...avai/predkladatel
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GAP106/10/1912), S
http://linked.open...iv/cisloPeriodika
  • 6
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 117601
http://linked.open...ai/riv/idVysledku
  • RIV/60461373:22340/13:43895650
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • transport; reconstruction; polyolefins; modelling; micro-tomography (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [EBCB957C885B]
http://linked.open...i/riv/nazevZdroje
  • Macromolecular Reaction Engineering
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 7
http://linked.open...iv/tvurceVysledku
  • Kosek, Juraj
  • Smolná, Klára
  • Štěpánek, František
  • Meisterová, Lucie
  • Zubov, Alexandr
http://linked.open...ain/vavai/riv/wos
  • 000320556700004
issn
  • 1862-8338
number of pages
http://bibframe.org/vocab/doi
  • 10.1002/mren.201300002
http://localhost/t...ganizacniJednotka
  • 22340
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