About: Hydrolysis of wheat B-starch and characterisation of acetylated maltodextrin     Goto   Sponge   NotDistinct   Permalink

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Description
  • Wheat B-starch was hydrolysed by alpha-amylase %22Liquozyme supra%22 from Bacillus licheniformis at 90 degrees C and pH 7. After 2 h, the dextrose equivalent was 18; according to size exclusion chromatography, however, the hydrolysate contained not only dominant malto-oligosaccharides with the degree of polymerisation (DP) { 10 but also more than 20% of components with DP higher than 40. The product was acetylated to a high degree as verified by FTIR and H-1 NMR (degree of substitution DS = 3.1); nevertheless, detailed analysis of the MALDI-TOF mass spectra of the product showed that most of the malto-oligosaccharides molecules contained one or two residual hydroxyls. Size exclusion chromatography confirmed that the acetylated maltodextrin still contained a significant part with DP } 40. This non-uniformity of acetylated maltodextrin, both with respect to DP and to DS, must be taken into account in the development of acetylated-maltodextrin applications such as use as plasticisers or compatibilisers in biodegradable composites.
  • Wheat B-starch was hydrolysed by alpha-amylase %22Liquozyme supra%22 from Bacillus licheniformis at 90 degrees C and pH 7. After 2 h, the dextrose equivalent was 18; according to size exclusion chromatography, however, the hydrolysate contained not only dominant malto-oligosaccharides with the degree of polymerisation (DP) { 10 but also more than 20% of components with DP higher than 40. The product was acetylated to a high degree as verified by FTIR and H-1 NMR (degree of substitution DS = 3.1); nevertheless, detailed analysis of the MALDI-TOF mass spectra of the product showed that most of the malto-oligosaccharides molecules contained one or two residual hydroxyls. Size exclusion chromatography confirmed that the acetylated maltodextrin still contained a significant part with DP } 40. This non-uniformity of acetylated maltodextrin, both with respect to DP and to DS, must be taken into account in the development of acetylated-maltodextrin applications such as use as plasticisers or compatibilisers in biodegradable composites. (en)
Title
  • Hydrolysis of wheat B-starch and characterisation of acetylated maltodextrin
  • Hydrolysis of wheat B-starch and characterisation of acetylated maltodextrin (en)
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  • Hydrolysis of wheat B-starch and characterisation of acetylated maltodextrin
  • Hydrolysis of wheat B-starch and characterisation of acetylated maltodextrin (en)
skos:notation
  • RIV/60461373:22330/13:43895673!RIV14-GA0-22330___
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  • P(GA525/09/0607), Z(AV0Z40500505)
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  • 1
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  • 78491
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  • RIV/60461373:22330/13:43895673
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  • gelatinization, polymers; mass-spektrometry; Uniformity; Acetylated maltodextrin; alpha-Amylase; Wheat B-starch (en)
http://linked.open.../riv/klicoveSlovo
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  • GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV
  • [FE67C3FB12B4]
http://linked.open...i/riv/nazevZdroje
  • Carbohydrate Polymers
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  • 98
http://linked.open...iv/tvurceVysledku
  • Horský, Jiří
  • Hrušková, Kateřina
  • Kruliš, Zdeněk
  • Netopilík, Miloš
  • Synytsya, Andriy
  • Walterová, Zuzana
  • Šárka, Evžen
  • Koláček, Jaroslav
  • Smrčková, Petra
http://linked.open...ain/vavai/riv/wos
  • 000325835600006
http://linked.open...n/vavai/riv/zamer
issn
  • 0144-8617
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.carbpol.2013.04.065
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  • 22330
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