About: Rapid method for simultaneous determination of PCBs, PBDEs and PAHs in fish samples

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Analytical methods for determination of various organic contaminants such as polychlorinated biphenyls (PCBs), polybrominated diphenyl ethers (PBDEs) and polyaromatic hydrocarbons (PAHs) in environmental and food matrices are typically based on multistep procedures that include Soxhlet extraction with a subsequent clean up and fractionation steps prior to relatively slow gas chromatography (GC) runs using either an electron capture (ECD) or a mass spectrometric (MS) detection in case of halogenated analytes, PAHs are commonly analysed separately using a liquid chromatography coupled to a fluorescence detector (LC-FLD), but for several non-flurescence PAHs including in the EFSA opinion, a GC-MS analysis is needed. In this study, the fast extraction and clean-up procedure of all mentioned pollutants from a fish fillet by a pressurised liquid extraction (PLE) has been tested. The main goal was to optimize an appropriate extraction/clean up procedure and to demonstrate the separation power of comprehensiv Analytical methods for determination of various organic contaminants such as polychlorinated biphenyls (PCBs), polybrominated diphenyl ethers (PBDEs) and polyaromatic hydrocarbons (PAHs) in environmental and food matrices are typically based on multistep procedures that include Soxhlet extraction with a subsequent clean up and fractionation steps prior to relatively slow gas chromatography (GC) runs using either an electron capture (ECD) or a mass spectrometric (MS) detection in case of halogenated analytes, PAHs are commonly analysed separately using a liquid chromatography coupled to a fluorescence detector (LC-FLD), but for several non-flurescence PAHs including in the EFSA opinion, a GC-MS analysis is needed. In this study, the fast extraction and clean-up procedure of all mentioned pollutants from a fish fillet by a pressurised liquid extraction (PLE) has been tested. The main goal was to optimize an appropriate extraction/clean up procedure and to demonstrate the separation power of comprehensiv (en)
Title	Rapid method for simultaneous determination of PCBs, PBDEs and PAHs in fish samples Rapid method for simultaneous determination of PCBs, PBDEs and PAHs in fish samples (en)
skos:prefLabel	Rapid method for simultaneous determination of PCBs, PBDEs and PAHs in fish samples Rapid method for simultaneous determination of PCBs, PBDEs and PAHs in fish samples (en)
skos:notation	RIV/60461373:22330/09:00022380!RIV10-MSM-22330___
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(7E08068), Z(MSM6046137305)
http://linked.open...iv/cisloPeriodika	6
http://linked.open...vai/riv/dodaniDat	2010
http://linked.open...aciTvurceVysledku	Čajka, Tomáš Hajšlová, Jana Pulkrabová, Jana Poustka, Jan
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Vysoká škola chemicko-technologická v Praze / Fakulta potravinářské a biochemické technologie
http://linked.open...dnocenehoVysledku	338115
http://linked.open...ai/riv/idVysledku	RIV/60461373:22330/09:00022380
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	PCBs; PAHs; PBDEs; GC; MS (en)
http://linked.open.../riv/klicoveSlovo	PBDEs GC MS PAHs PCBs
http://linked.open...odStatuVydavatele	AT - Rakouská republika
http://linked.open...ontrolniKodProRIV	[284E6F6B5024]
http://linked.open...i/riv/nazevZdroje	Organohalogen Compounds
http://linked.open...in/vavai/riv/obor	GM
http://linked.open...ichTvurcuVysledku	4 (xsd:int)
http://linked.open...cetTvurcuVysledku	6 (xsd:int)
http://linked.open...vavai/riv/projekt	CONtaminants in Food and Feed: Inexpensive DEtectioN for Control of Exposure
http://linked.open...UplatneniVysledku	2009
http://linked.open...v/svazekPeriodika	71
http://linked.open...iv/tvurceVysledku	Hajšlová, Jana Čajka, Tomáš Pulkrabová, Jana Drábová, Lucie Kalachová, Kamila Poustka, Jan
http://linked.open...n/vavai/riv/zamer	Teoretické základy potravinářských a biochemických technologií
issn	1026-4892
number of pages	6 (xsd:int)
http://localhost/t...ganizacniJednotka	22330
is http://linked.open...avai/riv/vysledek of	Rapid method for simultaneous determination of PCBs, PBDEs and PAHs in fish samples Rapid method for simultaneous determination of PCBs, PBDEs and PAHs in fish samples Rapid method for simultaneous determination of PCBs, PBDEs and PAHs in fish samples Rapid method for simultaneous determination of PCBs, PBDEs and PAHs in fish samples

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