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  • A simple and rapid multiresidue method for the determination of nine banned synthetic dyes in various spices has been developed. Reversed phase HPLC coupled with mass spectrometry (tandem in time - ion trap mass analyser) was employed for the examination of crude acetonitrile extract acidified with acetic acid. The detection limits of Para Red, Sudan Orange G, Sudan I, Sudan II, Sudan III, Sudan IV, Sudan Red 7B and Rhodamine B were in the range of 0.02-0.1 mg/kg, the recoveries ranged from 75.7 to 92.3% with repeatability of 0.9-11.3%. Rather worse performance characteristics were obtained with Tropaeolin 000, obviously due to its more polar nature as compared to other dyes involved in this study. In spite of that, the developed method can be used for a reliable control of a wide range of dyes used for illegal colouring of various spices.
  • A simple and rapid multiresidue method for the determination of nine banned synthetic dyes in various spices has been developed. Reversed phase HPLC coupled with mass spectrometry (tandem in time - ion trap mass analyser) was employed for the examination of crude acetonitrile extract acidified with acetic acid. The detection limits of Para Red, Sudan Orange G, Sudan I, Sudan II, Sudan III, Sudan IV, Sudan Red 7B and Rhodamine B were in the range of 0.02-0.1 mg/kg, the recoveries ranged from 75.7 to 92.3% with repeatability of 0.9-11.3%. Rather worse performance characteristics were obtained with Tropaeolin 000, obviously due to its more polar nature as compared to other dyes involved in this study. In spite of that, the developed method can be used for a reliable control of a wide range of dyes used for illegal colouring of various spices. (en)
Title
  • Determination of banned dyes in spices by liquid chromatography-mass spectrometry
  • Determination of banned dyes in spices by liquid chromatography-mass spectrometry (en)
skos:prefLabel
  • Determination of banned dyes in spices by liquid chromatography-mass spectrometry
  • Determination of banned dyes in spices by liquid chromatography-mass spectrometry (en)
skos:notation
  • RIV/60461373:22330/07:00022453!RIV10-MSM-22330___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(1P05OC057), Z(MSM6046137305)
http://linked.open...iv/cisloPeriodika
  • 25
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 416635
http://linked.open...ai/riv/idVysledku
  • RIV/60461373:22330/07:00022453
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Sudan dyes; Para Red; Rhodamine B; chilli; curry; liquid chromatography - mass spectrometry (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • CZ - Česká republika
http://linked.open...ontrolniKodProRIV
  • [12EFD814E9AE]
http://linked.open...i/riv/nazevZdroje
  • Czech Journal of Food Sciences
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...iv/tvurceVysledku
  • Hajšlová, Jana
  • Poustka, Jan
  • Botek, Petr
http://linked.open...ain/vavai/riv/wos
  • 000244286000002
http://linked.open...n/vavai/riv/zamer
issn
  • 1212-1800
number of pages
http://localhost/t...ganizacniJednotka
  • 22330
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