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| Description
| - Potential of ultra-performance liquid chromatography (UPLC) separation strategy coupled with tandem (in space) mass spectrometric detection (MS/MS) in multiresidue pesticide analysis was critically assessed. Performance parameters such as number of theoretical plates, height of theoretical plate, peak symmetry and peak capacity were measured/calculated on the basis of data generated by analysis of apple extracts containing 17 (semi)polar pesticides representing various classes of active ingredients of widely used crop protective preparations. Ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) procedure provided improved chromatographic parameters resulting in significantly increased sample throughput including lower solvent consumption and lower limits of quantitation (LOQs) for most of target analytes compared to common method employing conventional high-performance liquid chromatography (HPLC) separation.
- Potential of ultra-performance liquid chromatography (UPLC) separation strategy coupled with tandem (in space) mass spectrometric detection (MS/MS) in multiresidue pesticide analysis was critically assessed. Performance parameters such as number of theoretical plates, height of theoretical plate, peak symmetry and peak capacity were measured/calculated on the basis of data generated by analysis of apple extracts containing 17 (semi)polar pesticides representing various classes of active ingredients of widely used crop protective preparations. Ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) procedure provided improved chromatographic parameters resulting in significantly increased sample throughput including lower solvent consumption and lower limits of quantitation (LOQs) for most of target analytes compared to common method employing conventional high-performance liquid chromatography (HPLC) separation. (en)
- V článku je kriticky zhodnocena metoda extrémně účinné kapalinové chromatografie ve spojení s tandemovou hmotnostní spektrometrií (UPLC-MS/MS) v multireziduální analýze pesticidů. Parametry jako počet teoretických pater, výška teoretického patra, symetrie píku a kapacita píků byly měřeny pro 17 semipolárních pesticidů, které reprezentují různé skupiny aktivních složek ochranných prostředků plodin. Metoda UPLC-MS/MS poskytuje zlepšené chromatografické parametry, což zvyšuje produktivitu v sériové analýze včetně nižší spotřeby rozpouštědel a nižších kvantifikačních limitů ve srovnání s konvenční vysokoúčinnou kapalinovou chromatografií (HPLC). (cs)
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| Title
| - Ultra-Performance Liquid Chromatography - Tandem Mass Spectrometry (UPLC-MS/MS): A novel challenge in multiresidue pesticides analysis in food
- Extrémně účinná kapalinová chromatografie - tandemová hmotnostní spektrometrie (UPLC-MS/MS): Nová výzva v multireziduální analýze pesticidů v potravinách (cs)
- Ultra-Performance Liquid Chromatography - Tandem Mass Spectrometry (UPLC-MS/MS): A novel challenge in multiresidue pesticides analysis in food (en)
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| skos:prefLabel
| - Ultra-Performance Liquid Chromatography - Tandem Mass Spectrometry (UPLC-MS/MS): A novel challenge in multiresidue pesticides analysis in food
- Extrémně účinná kapalinová chromatografie - tandemová hmotnostní spektrometrie (UPLC-MS/MS): Nová výzva v multireziduální analýze pesticidů v potravinách (cs)
- Ultra-Performance Liquid Chromatography - Tandem Mass Spectrometry (UPLC-MS/MS): A novel challenge in multiresidue pesticides analysis in food (en)
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| skos:notation
| - RIV/60461373:22330/06:00017806!RIV07-MSM-22330___
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| http://linked.open.../vavai/riv/strany
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| http://linked.open...avai/riv/aktivita
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| http://linked.open...avai/riv/aktivity
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| http://linked.open...iv/cisloPeriodika
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| http://linked.open...vai/riv/dodaniDat
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| http://linked.open...aciTvurceVysledku
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| http://linked.open.../riv/druhVysledku
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| http://linked.open...iv/duvernostUdaju
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| http://linked.open...titaPredkladatele
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| http://linked.open...dnocenehoVysledku
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| http://linked.open...ai/riv/idVysledku
| - RIV/60461373:22330/06:00017806
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| http://linked.open...riv/jazykVysledku
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| http://linked.open.../riv/klicovaSlova
| - Ultra-performance liquid chromatography; High-performance liquid chromatography; Tandem mass spectrometry; Multiresidue; Pesticides; Food analysis (en)
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| http://linked.open.../riv/klicoveSlovo
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| http://linked.open...odStatuVydavatele
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| http://linked.open...ontrolniKodProRIV
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| http://linked.open...i/riv/nazevZdroje
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| http://linked.open...in/vavai/riv/obor
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| http://linked.open...ichTvurcuVysledku
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| http://linked.open...cetTvurcuVysledku
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| http://linked.open...UplatneniVysledku
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| http://linked.open...v/svazekPeriodika
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| http://linked.open...iv/tvurceVysledku
| - Hajšlová, Jana
- Kovalczuk, Tomáš
- Poustka, Jan
- Jech, Martin
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| http://linked.open...n/vavai/riv/zamer
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| issn
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| number of pages
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| http://localhost/t...ganizacniJednotka
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| is http://linked.open...avai/riv/vysledek
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