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  • Three different analytical procedures for the determination of DL-isocitric acid content in citrus fruit juices were compared. The DL-isocitric acid is an important marker in multicomponent procedures for the evaluation of authenticity and quality of fruit products. The compared procedures were the new proposed CITP procedure using coupled two capillaries, reverse phase HPLC method and enzymic procedure (Boehringer Mannheim). The optimised CITP electrolyte system was: 6 mM-HCl + 3.8 mM- BisTrisPropan + 2 mM-CaCl2 + 0.05% HPMC (LE) and 5 mM-MES + 1mM-BisTrisPropan (TE). The best correlation was found between the CITP and enzymic procedure (r = 0.956, n=6), the other cross correlation coefficients were 0.850 and 0.748 for HPLC - enzymic and HPLC - CITP respectively.
  • Three different analytical procedures for the determination of DL-isocitric acid content in citrus fruit juices were compared. The DL-isocitric acid is an important marker in multicomponent procedures for the evaluation of authenticity and quality of fruit products. The compared procedures were the new proposed CITP procedure using coupled two capillaries, reverse phase HPLC method and enzymic procedure (Boehringer Mannheim). The optimised CITP electrolyte system was: 6 mM-HCl + 3.8 mM- BisTrisPropan + 2 mM-CaCl2 + 0.05% HPMC (LE) and 5 mM-MES + 1mM-BisTrisPropan (TE). The best correlation was found between the CITP and enzymic procedure (r = 0.956, n=6), the other cross correlation coefficients were 0.850 and 0.748 for HPLC - enzymic and HPLC - CITP respectively. (en)
Title
  • Determination of isocitric acid content in fruit juices - detection of authenticity
  • Determination of isocitric acid content in fruit juices - detection of authenticity (en)
skos:prefLabel
  • Determination of isocitric acid content in fruit juices - detection of authenticity
  • Determination of isocitric acid content in fruit juices - detection of authenticity (en)
skos:notation
  • RIV/60461373:22330/02:00006868!RIV/2004/MSM/223304/N
http://linked.open.../vavai/riv/strany
  • 685-691
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM 223300004)
http://linked.open...iv/cisloPeriodika
  • 6
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 642730
http://linked.open...ai/riv/idVysledku
  • RIV/60461373:22330/02:00006868
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • isocitric, citric, juice, adulteration, HPLC, isotachophoresis (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [7EC21BE1599C]
http://linked.open...i/riv/nazevZdroje
  • J. Food Composition and Analysis
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...ocetUcastnikuAkce
http://linked.open...nichUcastnikuAkce
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 15
http://linked.open...iv/tvurceVysledku
  • Voldřich, Michal
  • Kvasnička, František
  • Vinš, I.
  • Pyš, P.
http://linked.open...n/vavai/riv/zamer
issn
  • 0889-1575
number of pages
http://localhost/t...ganizacniJednotka
  • 22330
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