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  • This study compares static headspace technique and methanol extraction/purge-and-trap analysis followed by thermal desorption/gas chromatography in attempts for quantification of gas survey results in the determination of these chemicals in soil. Several soils were contaminated with aqueous solution of perchloroethylene (PCE) (140 mg L-1) using a vapor treatment method. Soil spiking took place up to 24 h in desiccator by exposing individual soil samples contained in open 40 mL glass vials to PCE evaporated from the solution. After exposure the samples were stored and analyzed within 2 days. The achieved results strongly suggest that gas extraction can provide quantitative results, regarding PCE concentration in soils, which are not significantly different from liquid based extraction analysis.
  • This study compares static headspace technique and methanol extraction/purge-and-trap analysis followed by thermal desorption/gas chromatography in attempts for quantification of gas survey results in the determination of these chemicals in soil. Several soils were contaminated with aqueous solution of perchloroethylene (PCE) (140 mg L-1) using a vapor treatment method. Soil spiking took place up to 24 h in desiccator by exposing individual soil samples contained in open 40 mL glass vials to PCE evaporated from the solution. After exposure the samples were stored and analyzed within 2 days. The achieved results strongly suggest that gas extraction can provide quantitative results, regarding PCE concentration in soils, which are not significantly different from liquid based extraction analysis. (en)
Title
  • Comparison of perchloroethylene extraction techniques in soil gas survey quantification.
  • Comparison of perchloroethylene extraction techniques in soil gas survey quantification. (en)
skos:prefLabel
  • Comparison of perchloroethylene extraction techniques in soil gas survey quantification.
  • Comparison of perchloroethylene extraction techniques in soil gas survey quantification. (en)
skos:notation
  • RIV/60461373:22320/09:00022763!RIV10-MSM-22320___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM6046137308)
http://linked.open...iv/cisloPeriodika
  • 3
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 307749
http://linked.open...ai/riv/idVysledku
  • RIV/60461373:22320/09:00022763
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Soil; PCE; VOCs; Extraction; Gas survey; Vapor contamination (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [EE9069FC234D]
http://linked.open...i/riv/nazevZdroje
  • Central European Journal of Chemistry
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...iv/tvurceVysledku
  • Janků, Josef
  • Kubal, Martin
  • Zdravkov, Borislav
http://linked.open...ain/vavai/riv/wos
  • 000267239200002
http://linked.open...n/vavai/riv/zamer
issn
  • 1895-1066
number of pages
http://localhost/t...ganizacniJednotka
  • 22320
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