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  • In this work we described a simple method of CoO and Co3O4 nanoparticles synthesis with the tunable particle size. Nanoparticles were prepared by thermal decomposition of cobalt glycerolate in a controlled oxygen/nitrogen atmosphere for 1 h in the temperature range from 450 °C to 650 °C. Cobalt glycerolate was prepared by the reaction of cobalt nitrate with glycerol under reflux for 4 h. Obtained nanoparticles were analyzed by X-Ray diffraction to obtain information about their phase composition and average particle size, which was calculated using the Scherrer equation. Scanning electron microscopy and transmission electron microscopy were also used to confirm the particle sizes. Cobalt oxides nanoparticles with defined size can be prepared only by changing of the decomposition temperature of cobalt oxides precursors. The prepared nanoparticles can be used as sensors, in lithium-ion batteries, or in various nanoelectric devices.
  • In this work we described a simple method of CoO and Co3O4 nanoparticles synthesis with the tunable particle size. Nanoparticles were prepared by thermal decomposition of cobalt glycerolate in a controlled oxygen/nitrogen atmosphere for 1 h in the temperature range from 450 °C to 650 °C. Cobalt glycerolate was prepared by the reaction of cobalt nitrate with glycerol under reflux for 4 h. Obtained nanoparticles were analyzed by X-Ray diffraction to obtain information about their phase composition and average particle size, which was calculated using the Scherrer equation. Scanning electron microscopy and transmission electron microscopy were also used to confirm the particle sizes. Cobalt oxides nanoparticles with defined size can be prepared only by changing of the decomposition temperature of cobalt oxides precursors. The prepared nanoparticles can be used as sensors, in lithium-ion batteries, or in various nanoelectric devices. (en)
Title
  • CoO and Co3O4 nanoparticles with a tunable particle size
  • CoO and Co3O4 nanoparticles with a tunable particle size (en)
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  • CoO and Co3O4 nanoparticles with a tunable particle size
  • CoO and Co3O4 nanoparticles with a tunable particle size (en)
skos:notation
  • RIV/60461373:22310/14:43897128!RIV15-GA0-22310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA13-17538S), S
http://linked.open...iv/cisloPeriodika
  • 8
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 8918
http://linked.open...ai/riv/idVysledku
  • RIV/60461373:22310/14:43897128
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Nanocrystals; Thermal decomposition; Glycerolate; Cobalt oxides; Nanoparticles (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • BE - Belgické království
http://linked.open...ontrolniKodProRIV
  • [81E0419CB821]
http://linked.open...i/riv/nazevZdroje
  • Ceramics International
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 40
http://linked.open...iv/tvurceVysledku
  • Sofer, Zdeněk
  • Šimek, Petr
  • Sedmidubský, David
  • Huber, Štěpán
  • Jankovský, Ondřej
  • Bartůněk, Vilém
http://linked.open...ain/vavai/riv/wos
  • 000340328600137
issn
  • 0272-8842
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.ceramint.2014.04.082
http://localhost/t...ganizacniJednotka
  • 22310
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