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  • A new colorimetric detector tube for the detection of trace concentrations of nitrite in water was developed. The detector tube is based on a diazo coupling reaction of nitrite with dapsone and N-(1-naphthyl) ethylenediamine dihydrochloride during the formation of red-violet azo dye. Spherical granules (pellets) made from the composite material were used as the carrier of chemical reagents. They were prepared by pelletizing the mixture of microcrystalline cellulose, lactose, kaolin and polyvinylpyrrolidone. Colouring is done on a layer of silica gel impregnated with citric acid. The detector tube is highly sensitive, selective and stable when stored. The detection limit is 0.1 μg.ml–1, i.e. 0.03 μg.ml–1 N(NO2–). The optimal measuring range of nitrite concentration in the analyzed sample ranges from 0.5 to 80 μg.ml–1, i.e. 0.15—24.36 μg.ml–1 N(NO2–). The detector tube can easily be structurally modifi ed for analysis of nitrates with a detection limit of 1 μg/ml–1, i.e. 0.23 μg.ml–1 N(NO3–).
  • A new colorimetric detector tube for the detection of trace concentrations of nitrite in water was developed. The detector tube is based on a diazo coupling reaction of nitrite with dapsone and N-(1-naphthyl) ethylenediamine dihydrochloride during the formation of red-violet azo dye. Spherical granules (pellets) made from the composite material were used as the carrier of chemical reagents. They were prepared by pelletizing the mixture of microcrystalline cellulose, lactose, kaolin and polyvinylpyrrolidone. Colouring is done on a layer of silica gel impregnated with citric acid. The detector tube is highly sensitive, selective and stable when stored. The detection limit is 0.1 μg.ml–1, i.e. 0.03 μg.ml–1 N(NO2–). The optimal measuring range of nitrite concentration in the analyzed sample ranges from 0.5 to 80 μg.ml–1, i.e. 0.15—24.36 μg.ml–1 N(NO2–). The detector tube can easily be structurally modifi ed for analysis of nitrates with a detection limit of 1 μg/ml–1, i.e. 0.23 μg.ml–1 N(NO3–). (en)
Title
  • New detector tube for the detection of nitrite in water
  • New detector tube for the detection of nitrite in water (en)
skos:prefLabel
  • New detector tube for the detection of nitrite in water
  • New detector tube for the detection of nitrite in water (en)
skos:notation
  • RIV/60162694:G45__/11:00498724!RIV14-MO0-G45_____
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • I, P(VG20102013048)
http://linked.open...iv/cisloPeriodika
  • 1
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 91563
http://linked.open...ai/riv/idVysledku
  • RIV/60162694:G45__/11:00498724
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • detector tube; composite carrier; dapsone; N-(1-naphthyl) ethylenediamine dihydrochloride (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • SK - Slovenská republika
http://linked.open...ontrolniKodProRIV
  • [2B988B68DB8D]
http://linked.open...i/riv/nazevZdroje
  • Acta Chimica Slovaka
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 6
http://linked.open...iv/tvurceVysledku
  • Kobliha, Zbyněk
  • Pitschmann, Vladimír
  • Tušarová, Ivana
  • Vetchý, David
issn
  • 1337-978X
number of pages
http://localhost/t...ganizacniJednotka
  • G45
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