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Description
  • Titanium and its alloys are frequently used in many sectors, including the health care sector, where they outperform other materials. From the biocompatibility viewpoint, the preferred condition of these materials is ultrafine or nanostructured state. Processes based on severe plastic deformation (SPD) that are capable of producing microstructures with sizes of the order of nanometers are gaining importance these days. Their typical limitation is the small volume of material processed. One of available ways to enhancing the productivity is to combine the CONFORM continuous extrusion process with the ECAP method. This paper describes initial experience with this combined process in the CONFORM 315i machine, which is equipped with a specially-designed forming die chamber. Influence the number of passes through CONFORM machine on thermal stability was study by horizontal dilatometer and heat-flux calorimeter. The impact of deformation on the shift in recrystallization temperature of pure titanium was confirmed. The microstructure evolution and the grain growth behavior were investigated by electron back scattered diffraction (EBSD) technique. The deformed ultra fine-grained (UFG) titanium was annealed at a range of temperature (400-600 °C) for up to 6 h. The grain growth kinetics was characterized by calculating the grain growth activation energy Q and the time exponent n based on the experimental results for deformed material. Data for annealing temperatures of 550 and 600 °C allowed the values of the time exponent n = 0.19 and activation energy Q = 248 kJmol-1 were calculated.
  • Titanium and its alloys are frequently used in many sectors, including the health care sector, where they outperform other materials. From the biocompatibility viewpoint, the preferred condition of these materials is ultrafine or nanostructured state. Processes based on severe plastic deformation (SPD) that are capable of producing microstructures with sizes of the order of nanometers are gaining importance these days. Their typical limitation is the small volume of material processed. One of available ways to enhancing the productivity is to combine the CONFORM continuous extrusion process with the ECAP method. This paper describes initial experience with this combined process in the CONFORM 315i machine, which is equipped with a specially-designed forming die chamber. Influence the number of passes through CONFORM machine on thermal stability was study by horizontal dilatometer and heat-flux calorimeter. The impact of deformation on the shift in recrystallization temperature of pure titanium was confirmed. The microstructure evolution and the grain growth behavior were investigated by electron back scattered diffraction (EBSD) technique. The deformed ultra fine-grained (UFG) titanium was annealed at a range of temperature (400-600 °C) for up to 6 h. The grain growth kinetics was characterized by calculating the grain growth activation energy Q and the time exponent n based on the experimental results for deformed material. Data for annealing temperatures of 550 and 600 °C allowed the values of the time exponent n = 0.19 and activation energy Q = 248 kJmol-1 were calculated. (en)
Title
  • Study of thermal stability of ultra fine-grained commercially pure titanium wire prepared in conform equipment
  • Study of thermal stability of ultra fine-grained commercially pure titanium wire prepared in conform equipment (en)
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  • Study of thermal stability of ultra fine-grained commercially pure titanium wire prepared in conform equipment
  • Study of thermal stability of ultra fine-grained commercially pure titanium wire prepared in conform equipment (en)
skos:notation
  • RIV/26316919:_____/14:#0000526!RIV15-MSM-26316919
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(ED2.1.00/03.0077)
http://linked.open...iv/cisloPeriodika
  • 1.4.2014
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 48372
http://linked.open...ai/riv/idVysledku
  • RIV/26316919:_____/14:#0000526
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Conform- ECAP, Grain size growth rate, Recovery, Titanium (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • CH - Švýcarská konfederace
http://linked.open...ontrolniKodProRIV
  • [4906024A8FB5]
http://linked.open...i/riv/nazevZdroje
  • Materials Science Forum
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 782
http://linked.open...iv/tvurceVysledku
  • Dlouhý, Jaromír
  • Kubina, Tomáš
  • Kövér, Michal
  • Hodek, Josef
issn
  • 0255-5476
number of pages
http://bibframe.org/vocab/doi
  • 10.4028/www.scientific.net/MSF.782.415
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