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  • Purpose of this paper is to determine the temperatures of liquidus/solidus temperatures for multicomponent Fe-C-based alloys (industrially produced steel grades). The obtained results could be used in settings of conditions of steel casting and/or in the numerical simulations of processes occurring during casting and solidification of steel. Design/methodology/approach Two modern apparatus for dynamic thermal analysis were used. Measurements of liquidus/solidus temperatures were realized by two thermal analysis methods. Experiments by the differential scanning calorimetry were done using the new one Setaram Multi High Temperature Calorimeter with 3D sensor (smaller samples about 2.6 g). The direct thermal analysis was used for large samples (23 g) at the STA 449 F3 Jupiter equipment. Findings The differences between calculated and experimentally obtained values of liquidus/solidus temperatures were found. Also temperatures of solidification process are different than for “equilibrium” conditions.Research limitations/implications The obtained results are limited by the fact that range of realized experiments was devoted “only” to the two steel grades and only for “equilibrium” and for one cooling rate. The complexity of the solidification processes of such principally heterogeneous material (steel) needs to take into account much more aspect to quantify some leading dependencies of such processes. Practical implications Presented results will be implemented into steel production practice – lowering of superheating of steel during ingot casting. The obtained temperatures will be implemented also into numerical simulations of ingot solidification. Originality/value Two thermal analysis methods with different sample mass of steel was used under conditions of one research team. The direct cooperation between steel plant experts and university research team was applied. The utilization of results is the next phases of cooperated research of the authors.
  • Purpose of this paper is to determine the temperatures of liquidus/solidus temperatures for multicomponent Fe-C-based alloys (industrially produced steel grades). The obtained results could be used in settings of conditions of steel casting and/or in the numerical simulations of processes occurring during casting and solidification of steel. Design/methodology/approach Two modern apparatus for dynamic thermal analysis were used. Measurements of liquidus/solidus temperatures were realized by two thermal analysis methods. Experiments by the differential scanning calorimetry were done using the new one Setaram Multi High Temperature Calorimeter with 3D sensor (smaller samples about 2.6 g). The direct thermal analysis was used for large samples (23 g) at the STA 449 F3 Jupiter equipment. Findings The differences between calculated and experimentally obtained values of liquidus/solidus temperatures were found. Also temperatures of solidification process are different than for “equilibrium” conditions.Research limitations/implications The obtained results are limited by the fact that range of realized experiments was devoted “only” to the two steel grades and only for “equilibrium” and for one cooling rate. The complexity of the solidification processes of such principally heterogeneous material (steel) needs to take into account much more aspect to quantify some leading dependencies of such processes. Practical implications Presented results will be implemented into steel production practice – lowering of superheating of steel during ingot casting. The obtained temperatures will be implemented also into numerical simulations of ingot solidification. Originality/value Two thermal analysis methods with different sample mass of steel was used under conditions of one research team. The direct cooperation between steel plant experts and university research team was applied. The utilization of results is the next phases of cooperated research of the authors. (en)
Title
  • Study of Fe-C-Based alloys by dynamic methods of thermal analysis
  • Study of Fe-C-Based alloys by dynamic methods of thermal analysis (en)
skos:prefLabel
  • Study of Fe-C-Based alloys by dynamic methods of thermal analysis
  • Study of Fe-C-Based alloys by dynamic methods of thermal analysis (en)
skos:notation
  • RIV/25877950:_____/12:#0000055!RIV14-MPO-25877950
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  • P(ED0040/01/01), P(FR-TI3/243), P(GAP107/11/1566), S
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  • 2
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  • 172157
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  • RIV/25877950:_____/12:#0000055
http://linked.open...riv/jazykVysledku
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  • steel; solidification; thermal analysis; liquidus temperatures; solidus temperatures (en)
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  • PL - Polská republika
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  • [BADDB7951D9E]
http://linked.open...i/riv/nazevZdroje
  • Archives of Materials Science and Engineering
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  • 55
http://linked.open...iv/tvurceVysledku
  • Dobrovská, Jana
  • Gryc, Karel
  • Klus, Petr
  • Machovčák, Pavel
  • Michalek, Karel
  • Smetana, Bedřich
  • Socha, Ladislav
  • Tkadlečková, Markéta
  • Žaludová, Monika
issn
  • 1897-2764
number of pages
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